The Effect of Mineralizers on Synthesis of Perovskite-Phase Lanthanum Aluminate Powders

Article Preview

Abstract:

The solid-reaction was applied to synthesize perovskite-phase Lanthanum Aluminate powders by using AlOOH and La2(C2O4)3 as raw materials, mineralizer AlCl3 and AlF3 as the additives, graund and mixed, then calcined at 800°C and 1200°C for 3 h. The XRD pattern shows that mono-phase LaAlO3 powders can be obtained at 1200°C, and the SEM analysis indicates that the AlCl3 and AlF3 can promote the grain growth and have a good control of morphology.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

1241-1244

Citation:

Online since:

February 2011

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2011 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

[1] Li Lin, in: Application of High Temperature Superconducting Thin Films in Passive Microwave Devices. Physics, 2001, 30(7) 392-397.

Google Scholar

[2] National Key Basic Research Program Network, Research of the perovskite functional crystals, http: /www. 973. gov. cn: 80/show/stuff6-3. html.

Google Scholar

[3] Mao Shaoyu, Cai Yu and Liu Yao, et al in: Application of Oxalyl Dihydrazide in The Combustion Synthesis of LaAlO3, Functional Materials, 1998, 29(1): 110-111.

Google Scholar

[4] Xu Chaofen, Xu Yebin, in: Synthesis of Lanthanum Aluminate by Ethylene Diamine Tetraacetic Acid Gel Route, Journal of Huazhong University of Science and Technology (Natural Science), 2005, 33(1): 78-80.

Google Scholar

[5] Huang Guohua, Zhou Dongxiang and Xu Jianmei, et al in: Synthesis of Lanthanum Aluminate by the Liquid Mixing Method, Journal of Huazhong University of Science and Technology (Natural Science). 2004 32(02): 52-53.

Google Scholar

[6] Wang Xiuhui, Wu Xiaolin and Zhai Yuchun et al, in: The Synthesis of Lanthanum Aluminate Powders by Alkoxide-hydrolysis, Rare Metal Materials and Engineering. 2007. 8, 36(S1): 62-64.

Google Scholar

[7] Feng Duan, Shi Changxu et al, in: Introduction to Materials and Science [M], Beijing: Chemical Industry Press, (2002).

Google Scholar