Study on Nanometer ATO Powder Prepared with Citric Acid as Dispersant and its Conductive Properties

Abstract:

Antimony doped tin oxide (ATO) Nano powder was prepared by co-precipitation method, selecting SnCl4 • 5H2O and SbCl3 as the main raw material, citric acid as dispersant, ammonia solution (1:3) as precipitant, which was characterized, analyzed and tested by XRD, SEM, and digital conductivity meter. The optimum technological condition is that evenly-scattered powder whose crystalline structure is rutile, particle is sphere, size is about 10nm and conductivity is 1.32 ×102 µs/cm can be obtained when the reaction temperature is 60°C, Sb doping ratio is 10%, pH value is 2, calcinations temperature are 600°C and calcinations time are 2 hours.

• Periodical: Applied Mechanics and Materials (Volumes 599-601)
• Pages: 118-123
• DOI: https://doi.org/10.4028/www.scientific.net/AMM.599-601.118
• Online since: August 2014
• Authors: Xie Bin Zhu*, Jing Chen, Zhong Jia Huang
• Keywords: ATO, Citric Acid, Conductive Properties, Co-Precipitation Method, Preparation

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