The Study on Growth Interface of Floating Zone Silicon Crystal

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The shape and stability of growth interface have significant influence on the floating zone (for short FZ) silicon crystal. During the growth of crystal cone, growth interface reversal will happen due to the change of cooling mechanism, which makes crystal growth unstable. This impact will be more obvious for crystal with large diameter. During the growth of crystal body, with the crystal diameter increasing, the growth interface curvature and thermal stress both increase, which is easy to result in dislocation and even crack of the crystal. So this experiment mainly studied how to solve the instability problem due to interface inversion and how to reduce interface curvature. In the experiment we compared the growth interface shape of 6 inches <111> FZ silicon, at different pull speed, and find that during the growth of crystal cone, interface inversion can finish ahead with higher pull speed, and during the growth of crystal body, interface curvature decreased (interface depth≈32 mm) with lower pull speed ( υ=2.5mm/min) and higher rotate speed, to increases the chances for success of crystal growth.

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284-287

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September 2014

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© 2014 Trans Tech Publications Ltd. All Rights Reserved

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[1] T.F. Ciszek, T.H. Wang: Silicon Float-Zone Crystal Growth as a Tool for the Study of Defects and Impurities, To be presented at the Electrochemical Society Fall Conference Phoenix, Arizona October 22-27, (2000).

Google Scholar

[2] S.R. Coriell and M.R. Cordes, Contactless heater floating zone refining and crystal growth [J]. Crystal Growth 42(1977) 466.

DOI: 10.1016/0022-0248(77)90232-9

Google Scholar

[3] Mingxian Lin. Semiconductor material technology of silicon wafers [M]. TaiWan: All China books co., LTD, 2007. In Chinese.

Google Scholar

[4] A. Muiznieks, G. Raming, et al: Stress-induced dislocation generation in large FZ and CZ-silicon single crystals}numerical model and qualitative considerations[J]. Journal of Crystal Growth 230 (2001) 305–313.

DOI: 10.1016/s0022-0248(01)01322-7

Google Scholar

[5] Robert Menzel, Growth Conditions for Large Diameter FZ Si Single Crystals[D]. Berlin: der Technischen Universität Berlin, (2013).

Google Scholar

[6] Alfred Miihlbauer, Andris Muiznieks, et al: Interface shape, heat transfer and fluid flow in the floating zone growth of large silicon crystals with the needle-eye technique [J]. Journal of Crystal Growth 151 (1995) 66-79.

DOI: 10.1016/0022-0248(95)00027-5

Google Scholar

[7] Tetsuo Munakata, Ichiro Tanasawa. Study on silicon melt convection during the RF-FZ crystal growth process[J]. Journal of Crystal Growth 206 (1999) 23-26.

DOI: 10.1016/s0022-0248(99)00319-x

Google Scholar