Solid Phase Synthesis and Optical Properties of CdTiO3 Submicron Particles from Cd(OH)2 and P25 TiO2

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Abstract:

A simple and cost-effective low temperature (600 oC) solid phase method was proposed for the synthesis of CdTiO3 submicron particles, using Cd (OH)2 and P25 TiO2 as the starting materials. The composition and structure of the as-synthesized CdTiO3 submicron particles were characterized by X-ray diffraction and transmission electron microscopy. Besides, the optical properties of the as-synthesized CdTiO3 submicron particles were characterized by UV-vis diffuse reflection spectrum and photoluminescence spectrum.

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2868-2871

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January 2015

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© 2015 Trans Tech Publications Ltd. All Rights Reserved

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[1] B. Erjavec, R. Kaplan, P. Djinović and A. Pintar: Catalytic wet air oxidation of bisphenol A model solution in a trickle-bed reactor over titanate nanotube-based catalysts, Appl. Catal. B., 2013, 132-133, 342-352.

DOI: 10.1016/j.apcatb.2012.12.007

Google Scholar

[2] A. Turki, H. Kochkar, C. Guillard, G. Berhault and A. Ghorbel: Effect of Na content and thermal treatment of titanate nanotubes on the photocatalytic degradation of formic acid, Appl. Catal. B., 2013, 138-139, 401-415.

DOI: 10.1016/j.apcatb.2013.03.020

Google Scholar

[3] T. Kimijima, K. Kanie, M. Nakaya and A. Muramatsu: Solvothermal synthesis of SrTiO3 nanoparticles precisely controlled in surface crystal planes and their photocatalytic activity, Appl. Catal. B., 2014, 144, 462-467.

DOI: 10.1016/j.apcatb.2013.07.051

Google Scholar

[4] A.K. Nath and N. Medhi: Piezoelectric properties of environmental friendly bismuth doped barium titanate ceramics, Mater. Lett., 2012, 73, 75-77.

DOI: 10.1016/j.matlet.2011.12.113

Google Scholar

[5] J.O.H. Robles and C.A.R. González: Dielectric properties of Bismuth Titanate densified by Spark Plasma Sintering and Pressureless Sintering, J. Alloy. Comp., 2012, 536, S511-S515.

DOI: 10.1016/j.jallcom.2012.01.053

Google Scholar

[6] S.A. Paniagua, Y. Kim, K. Henry, R. Kumar and J.W. Perry: Surface-Initiated Polymerization from Barium Titanate Nanoparticles for Hybrid Dielectric Capacitors, ACS Appl. Mater. Interfaces, 2014, 6, 3477-3482.

DOI: 10.1021/am4056276

Google Scholar

[7] M.S. Hassan and T. Amna: Synthesis of High aspect ratio CdTiO3 nanofibers via electrospinning: characterization and photocatalytic activity, Ceram. Int., 2014, 40, 423-427.

DOI: 10.1016/j.ceramint.2013.06.018

Google Scholar

[8] C. Karunakaran and A. Vijayabalan: Electrical and optical properties of polyethylene glycol-assisted sol-gel solid state reaction-synthesized nanostructured CdTiO3, Mater. Sci. Semicond. Process., 2013, 16, 1992-(1996).

DOI: 10.1016/j.mssp.2013.07.032

Google Scholar

[9] B.J. Kennedy, Q. Zhou and M. Avdeev: The ferroelectric phase of CdTiO3: A powder neutron diffraction study, J. Solid State Chem., 2011, 184, 2987-2993.

DOI: 10.1016/j.jssc.2011.08.028

Google Scholar

[10] V. Gupta, K.K. Bamzai, P.N. Kotru and B.M. Wanklyn: Dielectric properties, ac conductivity and thermal behaviour of flux grown cadmium titanate crystals, Mater. Sci. Eng., B., 2006, 130, 163-172.

DOI: 10.1016/j.mseb.2006.03.006

Google Scholar

[11] Z. Imran, S.S. Batool, H. Jamil, M. Usman and M. Israr-Qadir: Excellent humidity sensing properties of cadmium titanate nanofibers, Ceram. Int., 2013, 39, 457-462.

DOI: 10.1016/j.ceramint.2012.06.048

Google Scholar

[12] Z. Imran, S.S. Batool, M.A. Rafiq, K. Rasool, M. Ahmad and R.N. Shahid: Investigation of Change in Surface Area and Grain Size of Cadmium Titanate Nanofibers upon Annealing and Their Effect on Oxygen Sensing, ACS Appl. Mater. Interfaces, 2014, 6, 4542-4549.

DOI: 10.1021/am500354a

Google Scholar

[13] Y.C. Zhang, G.L. Wang, X.Y. Hu and W.D. Zhou: Low-temperature solid-phase synthesis of pure CdTiO3 submicrocrystals using CdO2 nanoparticles as a precursor, J. Cryst. Growth., 2005, 285, 600-605.

DOI: 10.1016/j.jcrysgro.2005.09.008

Google Scholar

[14] L.Y. Yang, G.P. Feng, T.X. Wang and J.M. Zhang: Low temperature preparation and characterization of CdTiO3 nanoplates, Mater. Lett., 2011, 65, 2601-2603.

DOI: 10.1016/j.matlet.2011.05.090

Google Scholar

[15] J. Li, Y.C. Zhang, T.X. Wang and M. Zhang: Low temperature synthesis and optical properties of CaTiO3 nanoparticles from Ca(NO3)2·4H2O and TiO2 nanocrystals, Mater. Lett., 2011, 65, 1556-1558.

DOI: 10.1016/j.matlet.2011.03.031

Google Scholar