Hydroxyapatite Synthesized from Waste Eggshell via Ball Milling

Abstract:

Hydroxyapatite was synthesized using calcium originated from waste eggshell that was reacted with phosphate obtained from diammonium hydrogen orthophosphate by ball milling technique. The samples were mixed at different time from 5 to 150 min. The structure, function group and morphology of hydroxyapatite were characterized by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR) and field emission scanning electron microscopy (FE-SEM). The result showed that the hydroxyapatite phase was appeared after ball milling about 5 min and confirmed with FTIR results. The FE-SEM of hydroxyapatite powder was spherical shape and agglomerate. The crystallinity of hydroxyapatite was increased with increasing ball milling time. This experiment showed that the nano hydroxyapatite could synthesized from waste eggshell by ball milling technique.

• Periodical: Applied Mechanics and Materials (Volume 866)
• Pages: 12-16
• DOI: https://doi.org/10.4028/www.scientific.net/AMM.866.12
• Online since: June 2017
• Authors: Nisakorn Nuamsrinuan, Weeranuch Kaewwiset, Pichet Limsuwan, Kittisakchai Naemchanthara*
• Keywords: Ball Milling, Crystallinity, Eggshell, Hydroxyapatite

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