Study on Derivatising Condition of Cadaverine with Dansyl Chloride as Pre-Column Derivatising Agent

Xiao Yun Wang; Jin Sheng Feng; Hao Guo; Xiao Ying Tang

doi:10.4028/www.scientific.net/AMR.1073-1076.327

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HomeAdvanced Materials ResearchAdvanced Materials Research Vols. 1073-1076Study on Derivatising Condition of Cadaverine with...

Study on Derivatising Condition of Cadaverine with Dansyl Chloride as Pre-Column Derivatising Agent

Abstract:

A rapid ultrasonic wave-assisted dansylation procedure was developed for the derivatization of cadaverine prior to HPLC determination. Cadaverine was quantitatively dansylated in 10 min using a ultrasonic power of 200 W and a operating frequency of 40 KHz .In this case, the excellent derivatising condition are determined as follows: pH of buffer, 9.5; concentration of dansyl chloride, 5 mg/mL; time of reaction, 10 min. This method is fast, reproducible and practical for the analysis of cadaverine.

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Periodical:

Advanced Materials Research (Volumes 1073-1076)

Pages:

327-331

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.1073-1076.327

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Online since:

December 2014

Authors:

Xiao Yun Wang, Jin Sheng Feng*, Hao Guo, Xiao Ying Tang

Keywords:

Cadaverine, Dansylation, Optimization, Ultrasonic Wave-Assisted

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