Effect of Rice Husk Firing Temperature on Synthesis of Silica (SiO2)

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This paper presents the synthesis of silica (SiO2) from rice husk at different firing temperatures. Due to the environmental awareness and to reduce air pollution, agricultural wastes specifically rice husk is used to produce SiO2. Silica was prepared by washing with clean water without any chemical treatment. The rice husk was fired at 700, 800, 900, 1000, 1100 and 1200°C. In order to determine the effect of firing rice husk at different temperature, X-ray Diffraction (XRD) analyses were conducted. Crystalline silica were obtained at 1100°C and 1200°C firing temperature. At 900°C and 1000°C firing temperature, silica was observed to be in a transitional phase of amorphous into crystalline or it called as semi crystalline. However, at 700°C and 800°C silica remains to be in amorphous phases.

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470-474

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February 2015

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© 2015 Trans Tech Publications Ltd. All Rights Reserved

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[1] A. Onojah, A. N. Amah and I.M. Echi, Polymorphs of Crystalline Silica from Rice Husk Ash. Journal of Basic Physical Research, (2012) 73 -75.

Google Scholar

[2] R. Krishnarao, J. Subrahmanyam and T. J. Kumar, Studies on The Formation of Black Particles in Rice Husk Silica Ash. Journal of the European Ceramic Society, (2001) 99-104.

DOI: 10.1016/s0955-2219(00)00170-9

Google Scholar

[3] J. Nayak and J. Bera, Effect of Sintering Temperature on Phase-Formation Behavior and Mechanical Properties of Silica Ceramics Prepared From Rice Husk Ash. Phase Transitions, (2009) 879 - 888.

DOI: 10.1080/01411590903471564

Google Scholar

[4] Y. Shinohara and N. Kohyama, Quantitative Analysis of Tridymite and Cristobalite Crystallized in Rice Husk Ash by Heating. Industrial Health , (2004) 277-285.

DOI: 10.2486/indhealth.42.277

Google Scholar

[5] A. A. Boateng and D. A. Skeete, Incineration of Rice Husk for use as Cementitious Material:The Gunaya Experience. Cement and Concrete Research , (1990) 795-802.

DOI: 10.1016/0008-8846(90)90013-n

Google Scholar

[6] Y. Nakata, M. Suzuki, T. Okutani, M. Kikuchi and T. Akiyama, Preparation and Properties of SiO2 from Rice Husk. J Ceram Soc Japan , (1996) 842–849.

DOI: 10.2109/jcersj.97.842

Google Scholar

[7] C. Real, M. C. Alcala and J.M. Criado, Preparation of Silica from Rice Husks. J Am Ceram Soc , (1996) 2012-2016.

Google Scholar

[8] N. Hara, Utilization of Rice Husk Ash for Calcium Silicate Lightweight Building Materials. J Miner Soc Japan , (1988) 405-415.

Google Scholar

[9] M. Higuchi and Y. Azuma, Effect of Alkali Metal Oxide Addition on Crystallization and Phase Transformation of Sintered Spherical Silica. J Ceram Soc Japan , (1997) 385-390.

DOI: 10.2109/jcersj.105.385

Google Scholar

[10] A. M.Venezia, V. L. Parola, A. Longo and A. Martorana, Effect of Alkali Iions in The Amorphous to Crystalline Phase Transition of Silica. J Solid State Chem , (2001) 373-378.

DOI: 10.1006/jssc.2001.9345

Google Scholar

[11] L. A. Bui, C. Chen, C. Hwang and W. Wu, Effect of Silica Forms in Rice Husk Ah on The Properties of Concrete. International Journal of Minerals, Metallurgy and Materials, 252 (2012).

DOI: 10.1007/s12613-012-0547-9

Google Scholar

[12] E. P. Ayswarya, K. F. Francis, V. S. Renju and E. T. Thachil, Rice Husk Ash – A Valuable Reinforcement for High Density Polyethylene. Materials and Design, (2012) 1 – 7.

DOI: 10.1016/j.matdes.2012.04.035

Google Scholar

[13] D. R. Lee, Characterisation and The Diagenatic Transformation of Non and Micro-Crystalline Silica Minerals. Department of Earth and Ocean Sciences, University of Liverpool, (2005) 1- 20.

Google Scholar