For Libraries For Publication Open Access Downloads About Us Contact Us
Paper Titles
Evaluation of the Effect of Cooling Conditions and Heat Transfer Coefficients on Solidification of Al-Cu Binary Alloy in Static Casting Process
p.1
Study of α”-Martensitic Transformation in Ti35NbxSn Alloys Subjected to Cryogenic Heat Treatment
p.17
Susceptibility Study to Hydrogen Embrittlement of Welded Joints of API 5L X52 Steel in Sulphide Media
p.27
On the Inoculation and Phase Formation of Zr47.5Cu45.5Al5Co2 and Zr65Cu15Al10Ni10 Bulk Metallic Glass Matrix Composites
p.43
Experimental Study of Tensile and Flexural Strength of Cottonseed Hull Reinforced Epoxy Composites
p.99
Investigations on the Doping Effects on the Properties of Piezoelectric Ceramics
p.105
Study of Surface Roughness and MRR in Turning of SiC Reinforced Al Alloy Composite Using Taguchi Design Method, ANN and PCA Approach under MQL Cutting Condition
p.115
Earth Abundant Metals as Cost Effective Alternatives in Photocatalytic Applications: A Review
p.133
Evaluation of Steel Corrosion in Concrete Structures Using Impact-Echo Method
p.147

Study of α”-Martensitic Transformation in Ti35NbxSn Alloys Subjected to Cryogenic Heat Treatment

Article Preview

Abstract:

TiNbSn alloys have been extensively researched due to several properties they exhibit, including high mechanical strength, low elastic modulus, superelasticity, shape memory effect, biocompatibility. The present study evaluated the cryogenic heat treatment in the Ti35NbxSn alloys (x = 0.0; 2.5; 5.0; 7.5). The alloys were arc melted, cold formed and quenched in both water and liquid nitrogen at-198° C. The Ti35Nb2.5Sn alloy was also aged after exposed to both quenching medium. Microstructure and microhardness analyses were performed. Cryogenic treatment was not enough for transformation of primary β phase into martensitic α” in alloys containing 5 and 7.5% Sn. Cryogenic treatment provided β to α” transformation in alloys containing 0 and 2.5% Sn. The Sn-free alloy was more likely to α" transformation in both quenching medium. The alloys microhardness increased with decrease of both quenching temperature and Sn content. The increase of α" is also related to the increase of the alloy microhardness after aging.

You might also be interested in these eBooks
Advanced Materials and Technologies V View Preview

Info:

Periodical:

Advanced Materials Research (Volume 1158)

Pages:

17-26

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.1158.17

Citation:

Cite this paper

Online since:

April 2020

Authors:

Abraão Silva, Thiago Figueiredo Azevedo*, Weslley Rick Viana Sampaio, Luiz Carlos Pereira, Sandro Griza

Keywords:

Cryogenic Heat Treatment, Martensite, TiNbSn Alloys

Export:

RIS, BibTeX

Price:

Permissions CCC:

Request Permissions

Permissions PLS:

Request Permissions

Сopyright:

© 2020 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

* - Corresponding Author

References

[1] K. Miura, N. Yamada, S. Hanada e T. K. Jung, The bone tissue compatibilitty of a new Ti-Nb-Sn alloy with a low young´s modulus,, Acta Biomaterialia, vol. 7, pp.2320-2326, (2011).

DOI: 10.1016/j.actbio.2011.02.008

Google Scholar

[2] Y. L. Zhou e D. M. Lou, Microstructures and mechanical properties of Ti-Mo alloys cold-rolled and heat treated,,, Materials Caracterizations, vol. 62, pp.931-937, (2011).

DOI: 10.1016/j.matchar.2011.07.010

Google Scholar

[3] S. X. Liang, X. J. Feng, L. X. Yin, M. Z. Ma e R. P. Liu, Development of a new β Ti alloy with low modulus and favorable plasticity for implant material,, Materials Science and Engineering: C, vol. 61, pp.338-343, (2016).

DOI: 10.1016/j.msec.2015.12.076

Google Scholar

[4] Y. P. Hou, S. Guo, X. L. Qiao, T. Tian, Q. K. Meng, X. N. Cheng e X. Q. Zhao, Origin of ultralow Young׳s modulus in a metastable β-type Ti–33Nb–4Sn alloy,, Journal of the Mechanical Behavior of Biomedical Materials, vol. 59, pp.220-225, (2016).

DOI: 10.1016/j.jmbbm.2015.12.037

Google Scholar

[5] Y. L. Hao, S. J. Li, S. Y. Sun e R. Yang, Effect of Zr and Sn on Young's modulus and superelasticity of Ti-Nb-based alloys,, Materials Science Engineering A, vol. 441, pp.112-118, (2006).

DOI: 10.1016/j.msea.2006.09.051

Google Scholar

[6] M. Niinomi, M. Nakai e J. Hieda, Development of new metallic alloys for biomedical applications,, ACTA BIOMATERIALIA, vol. 8, nº 11, pp.3888-3903, (2012).

DOI: 10.1016/j.actbio.2012.06.037

Google Scholar

[7] Y. F. Zheng, B. L. Wang, J. G. Wang e L. C. Zhao, Corrosion behavior of Ti-Nb-Sn shape memory alloys in different simulated body solutions,, Materials Science and Engineering A, vol. 438, pp.891-895, (2006).

DOI: 10.1016/j.msea.2006.01.131

Google Scholar

[8] Thiago Figueiredo Azevedo, Carlos Eduardo Celestino de Andrade, Silvando Vieira dos Santos, Abraão Santos Silva, SandroGriza, Fatigue and corrosion-fatigue strength of hot rolled Ti35Nb2.5Sn alloy, Materials & Design Volume 85, 15 November 2015, Pages 607-612.

DOI: 10.1016/j.matdes.2015.07.045

Google Scholar

[9] Thiago Figueiredo Azevedo, Tiago Nunes Lima, Juan Garcia de Blas, Luiz Carlos Pereira, Sandro Griza, The mechanical behavior of TiNbSn alloys according to alloying contents, cold rolling and aging, Journal of the Mechanical Behavior of Biomedical Materials, Volume 75, 2017, Pages 33-40.

DOI: 10.1016/j.jmbbm.2017.07.002

Google Scholar

[10] Cristyane Silva Santos de Oliveira, Sandro Griza, Marize Varella de Oliveira, Alexandre Antunes Ribeiro, Mônica Barreto Leite, Study of the porous Ti35Nb alloy processing parameters for implant applications, Powder Technology, Volume 281, 2015, Pages 91-98.

DOI: 10.1016/j.powtec.2015.03.014

Google Scholar

[11] Cristyane Silva Santos de Oliveira, Alexandre Antunes Ribeiro, Alexandre Antunes Ribeiro, Roseli Marins Balestra, Sandro Griza, Marize Varella de Oliveira, Characterization of Porous Ti-35Nb Alloy Sintered at Different Temperatures for Implant Applications, Materials Science Forum, 2014, v. 802, pp.496-500.

DOI: 10.4028/www.scientific.net/msf.802.496

Google Scholar

[12] N.Masahashia, Y.Mori, H.Tanaka, A.Kogure, H.Inoue, K.Ohmura, Y.Kodama, M.Nishijima, E.Itoi, S.Hanada, Bioactive TiNbSn alloy prepared by anodization in sulfuric acid electrolytes, Materials Science and Engineering: C, Volume 98, May 2019, Pages 753-763.

DOI: 10.1016/j.msec.2019.01.033

Google Scholar

[13] S. Griza, D. H. G. d. S. Sá, W. W. Batista, J. C. G. d. Blas e L. C. Pereira, Microstructure and mechanical properties of hot rolled TiNbSn alloys,, Materials and Design, vol. 56, pp.200-208, (2014).

DOI: 10.1016/j.matdes.2013.10.067

Google Scholar

[14] D. H. Ping, C. Y. Cui, F. X. Yin e Y. T. Yamabe-Mitarai, Investigation on martensite in a Ti-Nb-Based shape memory alloy,, Scripta Materialia, vol. 54, pp.1305-1310, (2006).

DOI: 10.1016/j.scriptamat.2005.12.022

Google Scholar

[15] P. Laheurte, F. Prima, A. Eberhardt, T. Gloriant, M. Wary e E. Patoor, Mechanical properties of low modulus β titanium alloys designed from the electronic approach,, Journal of the Mechanical Behavior of Biomedical Materials , vol. 3, pp.565-573, (2010).

DOI: 10.1016/j.jmbbm.2010.07.001

Google Scholar

[16] T. Ozaki, H. Matsumoto, S. Watanabe e S. Hanada, Beta Ti Alloys with Low Young's Modulus,, Materials Transaction, vol. 45, nº 8, pp.2776-2779, (2004).

DOI: 10.2320/matertrans.45.2776

Google Scholar

[17] C. A. F. Salvador, E. S. N. Lopes, C. A. Ospina e R. Caram, Orthorhombic martensite formation upon aging in a Ti-30Nb-4Sn alloy,, Materials Chemistry and Physics, vol. 183, pp.238-246, (2016).

DOI: 10.1016/j.matchemphys.2016.08.023

Google Scholar

[18] H. Matsumoto, S. Watanabe e S. Hanada, Beta TiNbSn alloys with low young's modulus and high strength,, Materials Transactions, vol. 46, pp.1070-1078, (2005).

DOI: 10.2320/matertrans.46.1070

Google Scholar

[19] H. Matsumoto, S. Watanabe e S. Hanada, Microstructures and mechanical properties of metastable β TiNbSn alloys cold rolled and heat treated,, Journal of Alloys and Compounds, vol. 439, pp.145-155, (2007).

DOI: 10.1016/j.jallcom.2006.08.267

Google Scholar

[20] Taek-Kyun Junga, Hyo-Soo Lee, Satoshi Semboshi, Naoya Masahashi, Tadasu Abumiya, Shuji Hanada, A new concept of hip joint stem and its fabrication using metastable TiNbSn alloy, Journal of Alloys and Compounds 536S (2012) S582–S585.

DOI: 10.1016/j.jallcom.2011.12.077

Google Scholar

[21] Qu, W.T.; Sun, X.G.; Yuan, B.F.; Xiong, C.Y.; Zhang, F.; Li, Y.; Sun, B.H. Microstructures and phase transformations of Ti–30Zr–xNb (x = 5, 7, 9, 13 at.%) shape memory alloys. Materials. Characterization. Vol. 122, p.1–5; (2016).

DOI: 10.1016/j.matchar.2016.10.019

Google Scholar

[22] G. R. Li, J. F. Cheng, H. M. Wang e C. Q. Li, The influence of cryogenic-aging circular treatment on the microstructure and properties of aluminum matrix composites,, Journal of Alloys and Compounds, vol. 695, pp.1930-1945, (2017).

DOI: 10.1016/j.jallcom.2016.11.028

Google Scholar

[23] H. Li, W. Tong, J. Cui, L. Chen e L. Zuo, The influence of deep cryogenic treatment on the properties of high-vanadium alloy steel,, Materials Science and Engineering: A, vol. 662, pp.356-362, (2016).

DOI: 10.1016/j.msea.2016.03.039

Google Scholar

[24] S. Kumar, A. Batish, R. Singh e T. Singh, Machining performance of cryogenically treated Ti–5Al–2.5Sn titanium alloy in electric discharge machining: A comparative study,, Journal of Mechanical Engineering Science, (2016).

DOI: 10.1177/0954406215628030

Google Scholar

[25] L. Y. Xu, J. Zhu, H. Y. Jing, L. Zhao, X. Q. Lv e Y. D. Han, Effects of deep cryogenic treatment on the residual stress and mechanical properties of electron-beam-welded Ti–6Al–4V joints,, Materials Science and Engineering: A, vol. 673, pp.503-510, (2016).

DOI: 10.1016/j.msea.2016.07.101

Google Scholar

[26] L. Y. Xu, J. Zhu, H. Y. Jing, X. Q. Lv e Y. D. Han, Effects of deep cryogenic treatment on the residual stress and mechanical properties of electron-beam-welded Ti-6Al-4V joints,, Materials Science & Engineering A, vol. 673, pp.503-510, (2016).

DOI: 10.1016/j.msea.2016.07.101

Google Scholar

[27] T. S. Vinothkumar, D. Kandaswamy, G. Prabhakaran e A. Rajadurai, Microstructure of cryogenically treated martensitic shape memory nickel-titanium alloy,, Journal of Conservative Dentistry, vol. 18, pp.292-296, (2015).

DOI: 10.4103/0972-0707.159727

Google Scholar

[28] A. Helth, S. Pilz, T. Kirsten, L. Giebeler, J. Freudenberger, M. Calin, J. Eckert e A. Gebert, Effect of thermomechanical processing on the mechanical biofunctionality of a low modulus Ti-40Nb alloy,, Journal of the Mechanical Behavior of Biomedical Materials., vol. 65, pp.137-150, (2017).

DOI: 10.1016/j.jmbbm.2016.08.017

Google Scholar

[29] K. Gu, J. Wang e Y. Zhou, Effect of cryogenic treatment on wear resistance of Ti–6Al–4V alloy for biomedical applications,, journal of the mechanical behavior of biomedical materials, vol. 30, pp.131-139, (2014).

DOI: 10.1016/j.jmbbm.2013.11.003

Google Scholar

© 2025 Trans Tech Publications Ltd. All rights are reserved, including those for text and data mining, AI training, and similar technologies. For open access content, terms of the Creative Commons licensing CC-BY are applied.
Scientific.Net is a registered trademark of Trans Tech Publications Ltd.