The Effect of Power Rate Microwave Heating on Limestone Carbonated Hydroxyapatite Scaffold Using Gas Foaming Method

Abstract:

Microwave heating was used with a gas foaming method for fabricating limestone carbonated hydroxyapatite scaffold (SCHA). Carbonated hydroxyapatite (CHA) was produced from limestone as a calcium source using the co-precipitation method. For further treatment, 0.6 gr CHA powder was mixed in 1 ml H₂O₂ solution as a blowing agent. The slurry-foam-like CHA was heated in a microwave with different levels of heating power from 180 W to 720 W. The SCHA samples were characterized using X-ray diffraction (XRD), Fourier-transform infrared (FTIR), and Scanning electron microscope (SEM). The crystallinity and crystallite size were affected due to different rates of heating power in the microwave-assisted method. The increasing temperature decreased the crystallite size from 37.49 to 33.97(nm). However, other crystallinity trends were observed at 180 W because the lower power heating needed a longer time to be formed SCHA. The different power rates have an insignificant contribution to the morphology of the scaffolds.

• Periodical: Advanced Materials Research (Volume 1179)
• Pages: 11-18
• DOI: https://doi.org/10.4028/p-6Gy5GL
• Online since: January 2024
• Authors: Dyah Aris Widyastuti*, Yusril Yusuf
• Keywords: Carbonated Hydroxyapatite, Gas Foaming, Limestone, Microwave-Assisted, Scaffold

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