Synthesis and Characterization of 3Y-TZP Powders by Stirring Ball Milling

Da Guang Li; Zhi Wu; Chun Yang Pan; Wei Qin Fu; Qiu Hong Wang

doi:10.4028/www.scientific.net/AMR.239-242.2790

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HomeAdvanced Materials ResearchAdvanced Materials Research Vols. 239-242Synthesis and Characterization of 3Y-TZP Powders...

Synthesis and Characterization of 3Y-TZP Powders by Stirring Ball Milling

Abstract:

3 mol% yttric(Y₂O₃)-stabilized tetragonal zirconia ( denoted as: 3Y-TZP) powders were synthesized by the reaction of Zr(CO₃)₂·nH₂O,Y₂(C₂O₄)₃·nH₂O,H₂C₂O₄·2H₂Oand H₄C₂O₂-C₂H₅OH mixed via stirring ball milling. The curve of decomposition of precursors was studied according to differential thermal analysis and thermogravimetry (DTA-TG). The 3Y-TZP powders were confirmed by characterization of XRD, TEM and BET. These results shown that the size of the 3Y-TZP powders were in the range of about 18nm-28nm with good dispersion and the main phase of target production was tetragonal phase. When calcining temperature and holding time was higher, the size of particles grown up and the tetragonal phase volume fraction decrease gradually. And the calcining temperature has more significant effect.

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Periodical:

Advanced Materials Research (Volumes 239-242)

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2790-2794

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.239-242.2790

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May 2011

Authors:

Da Guang Li, Zhi Wu, Chun Yang Pan, Wei Qin Fu, Qiu Hong Wang

Keywords:

3Y-TZP, Characterization, Precursor, Stirring Ball Milling

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