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HomeAdvanced Materials ResearchAdvanced Materials Research Vols. 295-297Synthesis of VO2(A) Nanostructures by a...

Synthesis of VO₂(A) Nanostructures by a Hydrothermal Method and their Transition to VO₂(M)

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Abstract:

VO₂(A) nanobelts have been synthesized using V₂O₅, H₂O₂, ethanol, H₂O as the starting materials through a facile hydrothermal method. The as-obtained products were characterized by X-ray powder diffraction (XRD), X-ray photoelecton spectroscopy (XPS), transmission electron microscopy (TEM) and differential scanning calorimetry (DSC). Some parameters, such as, the reaction time, reaction temperature and the ratio of EtOH/H₂O, have greatly influenced on the phases and morphologies of the final products. It was found that VO₂(A) can be converted to VO₂(M) at 700 °C for 2 h for the first time. Furthermore, the phase transition properties of VO₂(A) and VO₂(M) phases were respectively studied.

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Manufacturing Science and Technology, AEMT2011

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Periodical:

Advanced Materials Research (Volumes 295-297)

Pages:

368-372

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.295-297.368

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Online since:

July 2011

Authors:

Ya Lan Zhong, Yi Fu Zhang, Xin Liu, Xing Hai Liu, Chi Huang, Hou Bin Li

Keywords:

Hydrothermal Method, Nanomaterial, Phase Transition, Vanadium Oxides, VO₂(a), VO₂(m)

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© 2011 Trans Tech Publications Ltd. All Rights Reserved

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