The Synthesis of Novel Chiral Organic Light-Emitting Material: 2R,3R-Di(tert-Butanesulfiny)Thiophene

Article Preview

Abstract:

A mide, simple and efficient synthetic procedure for the preparation of 2,3-di(tert-butanesulfiny)Thiophene and key intermediates, chiral tert-Butanethiosulfinate have been developed. The procedure described herein offers several advantages, including high product yields, easy purification, and large scale production. 2,3-di(tert-butanesulfiny)Thiophene has good solubility in organic solvents.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

151-154

Citation:

Online since:

September 2011

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2011 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

[1] (a) Wu, C.-C.; Lin, Y.-T.; Wong, K.-T.; Chen, R.-T.; Chien, Y.-Y. Adv. Mater. 2004, 16, 61.(b) Su, H.-J.; Wu, F.-I.; Shu, C.-F. Macromolecules 2004, 37, 7197. (c) Wu, Y.; Li, J.; Fu, Y.; Bo, Z. Org. Lett. 2004, 6, 3485. (d) Cao, X.-Y.; Zhang, W.; Zi, H.; Pei, J. Org. Lett. 2004, 6, 4845. (e) Wong, K.-T.; Chen, R.-T.; Fang, F.-C.; Wu, C.-C.; Lin, Y.-T. Org. Lett. 2005, 7, 1979.

DOI: 10.1021/ol048709o

Google Scholar

[2] (a) Heredia, D.; Natera, J.; Gervaldo, M.; Otero, L.; Fungo, F.; Lin, C. Y.; Wong, K. T. Org. Lett. 2009, 12, 12. (b) Chi, L. C.; Hung, W. Y.; Chiu, H. C.; Wong, K. T. Chem. Commun. 2009, 3892.

DOI: 10.1021/ol902314z

Google Scholar

[3] Wu, C. C.; Liu, T. L.; Hung, W. Y.; Lin, Y. T.; Wong, K. T.; Chen, R. T.; Chen, Y. M.; Chien, Y. Y. J. Am. Chem. Soc. 2003, 25, 3710.

Google Scholar

[4] Lyu, Y. Y.; Kwak, J.; Jeon, W. S.; Byun, Y.; Lee, H. S.; Kim, D.; Lee, C.; Char, K. AdV. Func. Mater. 2009, 19, 420.

Google Scholar

[5] Sun, X.-X.; Li, Y.-C.; Liu, X. –M.; Zhuang, X. –X.; Lou, Y. -Zh. Advanced Materials Research 2011, 287-290, 270.

Google Scholar