Study on Synthesis of Nesquehonite Whiskers

Article Preview

Abstract:

Thermal composition of low temperature water is taken as way in the text, with the MgSO4•7H2O and NH4HCO3 being raw materials to make nesquehonite whiskers, further talking about the concentration of the reactant, reactive temperatures, mixing speed, solution pH and the quantity of additive addition etc. factors impacting whiskers synthetic of magnesium carbonate hydrate by controlling the growth environment. On this foundation ,finally drop MgSO4 solutions by 2.45 mL/min at 50oC by 0.5 mol/L. Join 0.5% KH2PO4 obtain slender perfectly straight, smooth surface and average length-diameter ratio of 34 crystal whiskers, carrying out the control to the crystal whiskers facial look and optimized performance for 247 μm and average diameter for 7.2 μm and on the average long diameter comparing.

You might also be interested in these eBooks

Info:

Periodical:

Advanced Materials Research (Volumes 361-363)

Pages:

332-336

Citation:

Online since:

October 2011

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2012 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

[1] C C Evans.Whiskers[M],Mills Boon Limited.London.1972:10.

Google Scholar

[2] LiWu. Inorganic whisker [M],Chemical Industry Press.2005:1-2.In Chinese.

Google Scholar

[3] PingkeYan, ZhengxianMa, YujuanGao.China Non-metallic Mining Industry Herald,2009:23-25. In Chinese.

Google Scholar

[4] Kloprogge J T,Martens W N,Nothdurft L,et al.Low Temperature Synthesis and Characterization of Nesquehonite [J].J.Mater.Sci.Lett.,2003,22(11):825-829.

Google Scholar

[5] Mitsuhashi K,Tagami N,Tanabe K,et al.Synthesis of Microtubes with a Surface of "House of Cards"StructureviaNeedlelikeParticlesandControlofTheirPoreSize[J].Langmuir,2005,21:3659-3663.

DOI: 10.1021/la047580o

Google Scholar

[6] Wanping Wang, Yi Zhang. Journal of the Chinese Ceramic Society, Vol.30 (2002),pp.93-95. In Chinese.

Google Scholar

[7] X L WANG, D F XUE.Mater Lett,2006,60(25-26):3160-3164. In Chinese.

Google Scholar

[8] Y Wang, Z B Li. J.Cryst.Growth,2008,310:1220-1227. In Chinese.

Google Scholar

[9] X X Yan, Y F Li, D F Xue,et al. Bonding Analysis on the Crystallization of Magnesium Carbonate Hydrate[J].J. Synthetic Cryatals, 2007,365(5):991-999. In Chinese.

Google Scholar