Reactive Divided Wall Distillation Column: Simulation and Experiment of Methyl Acetate Hydrolysis

Abstract:

As a combination of divided wall column (DWC) and reactive-distillation column, the reactive divided wall distillation column is a highly complex technology that reaction and separation can occur simultaneously, which can reduce the energy consumption and decrease the costs of captial and operation. This new process was simulated with PROⅡ software and mini plant experiments were implemented. In addition, we investigated the influences of reflux ratio, liquid distribution ratio and molar ratio of ester in water on the conversion rate of methyl acetate and the purity of the product respectively. It could be seen that the trend from experiments was suitable with simulation results.

• Periodical: Advanced Materials Research (Volumes 468-471)
• Pages: 2785-2789
• DOI: https://doi.org/10.4028/www.scientific.net/AMR.468-471.2785
• Online since: February 2012
• Authors: Yan Wang, He Xu Ma, Huai Gong Zhu, Wei Tang
• Keywords: Energy Consumption (EC), Hydrolysis, Reactive Divided Wall Distillation Column

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