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Synthesis of Titania Microshperes with Controllable Diameter Under Solvothermal Conditions

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Abstract:

Bead-structured titanium dioxide microspheres were successfully prepared by a facile one-step solvothermal method using diblock copolymers poly(ethylene oxide)-block-polystyene (PEO-b-PS) as the structure-directing agent. The products were characterized by scanning electron microscopy, thermogravimetic analysis and X-ray powder diffraction (XRD) technique. The XRD patterns show that the products synthesized with low content of HCl are anatase titanium dioxide and the products synthesized with low content of HCl are rulite titanium dioxide.

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Periodical:

Advanced Materials Research (Volumes 476-478)

Pages:

1678-1681

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.476-478.1678

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Online since:

February 2012

Authors:

Dong Bo Guo, Yan Ping Wang, Xiao Chao Zhang, Jia Wang, Yi Min Wang

Keywords:

Block-Copolymer, Solvothermal Method, Structure-Directing Agent, TiO2 Microspheres

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© 2012 Trans Tech Publications Ltd. All Rights Reserved

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