Solvothemal Synthesis and Characterization of α-MnS Micronsized Architectures

Rong Wu; Le Tian Tao; Ji Kang Jian

doi:10.4028/www.scientific.net/AMR.486.309

Paper Titles

A Service Life Prediction for Waste Disposal Facility Concrete Exposed to Chloride Attack
p.284

Effects of Antibacterial Treatment Temperature on the Properties of Copper-Bearing Antibacterial Duplex Stainless Steels
p.289

The Precipitation and Dissolution of Alloy Iron Carbides in Vacuum Carburization Processes for Automotive and Aircraft Applications - Part I
p.297

The Precipitation and Dissolution of Alloy Iron Carbides in Vacuum Carburization Processes for Automotive and Aircraft Applications - Part II
p.303

Solvothemal Synthesis and Characterization of α-MnS Micronsized Architectures
p.309

Finite Element and Experimental Investigation of Human Femur Cortical Bone Microdamage during Radial Fretting
p.313

Corrosion Behavior of Zr-Based Bulk Metallic Glasses by Addition of Ni
p.321

Epoxidation of Soybean Oil with Tert-Butyl Hydroperoxide over Manganese (III) Tetraphenylporphyrin Chloride Catalyst
p.328

Continuous Sheet Metal Forming - A Linearly Incremental Forming Method for Manufacturing 3D Surface Parts
p.334

HomeAdvanced Materials ResearchAdvanced Materials Research Vol. 486Solvothemal Synthesis and Characterization of...

Solvothemal Synthesis and Characterization of α-MnS Micronsized Architectures

Abstract:

Mixed solvent of ethylenediamine (EDA) and ethylene glycol (EG) using MnCl4H₂O, and (NH₂)₂CS as precursors was used to synthesize α-MnS micronsized architectures. Optimal α-MnS crystals were successfully grown from a mixed solvent of EDA:EG with a volume ratio of 1:1, reaction temperature of 140-180 °C and maintained for 6h. X-ray diffraction (XRD), scanning electron microscopy (SEM) was employed to characterize the structure and morphology of the product. The results show that the morphologies of α-MnS are found to be temperature dependent.