Effects of Calcination Temperature on Electrospun Silica Fibers

Nuttaya Pramuansub; Piyada Jittangprasert; Panitarn Wanakamol

doi:10.4028/www.scientific.net/AMR.488-489.602

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HomeAdvanced Materials ResearchAdvanced Materials Research Vols. 488-489Effects of Calcination Temperature on Electrospun...

Effects of Calcination Temperature on Electrospun Silica Fibers

Abstract:

Silica fibers have been fabricated via sol-gel reaction and electrospinning. The precursor solution was prepared from tetraethyl-orthosilicate (TEOS), ethanol and aqueous hydrochloric acid. The viscous solution was electrospun at 15kV applied voltage and 20 cm tip-to-collector distance. The process yielded nonwoven sheet of silica fibers with good mechanical integrity. The silica fiber specimens were calcined at different temperatures: 400°C, 600°C and 800°C. Scanning electron microscope (SEM) observation reveals smooth and long fibers with average diameter below 0.5μm for all samples, both as spun and calcined. Fourier transform infrared spectroscopy (FT-IR) spectra show effects of calcination temperature on chemical structure of the fibers. Calcination results in the removal of organic residuals and leaving mostly silica content

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Periodical:

Advanced Materials Research (Volumes 488-489)

Pages:

602-606

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https://doi.org/10.4028/www.scientific.net/AMR.488-489.602

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Online since:

March 2012

Authors:

Nuttaya Pramuansub, Piyada Jittangprasert, Panitarn Wanakamol

Keywords:

Calcination, Electro-Spinning, Silica Fibers

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References

[1] Huang, Z., Zhang, Y.Z., Kotaki, M. and Ramakrishna, S: Compos. Sci. Technol. 2003, 63(15), pp.2223-2253.

Google Scholar

[2] Rutledge, G.C. and Fridrikh, S. V: Adv. Drug Delivery Rev. 2007, 59(14), pp.1384-1391.

Google Scholar

[3] R. Furlan, E.W. Simoes, M.L.P. da Silva, I. Ramos, E. Fachini: Polymer 48 (2007) pp.5107-5115.

Google Scholar

[4] J. Kim, G. Cheruvally, X. Li, J. Ahn, K. Kim, H. Ahn: J. Power Sources 178 (2008) p.815–820.

DOI: 10.1016/j.jpowsour.2007.08.063

Google Scholar

[5] L. Ji and X. Zhang: Mater. Lett. 62 (2008) p.2161 –2164.

Google Scholar

[6] Yiyang Zhao, Haiying Wang, Xiaofeng Lu, Xiang Li, Yang Yang, Ce Wang: Mater. Lett. 62 (2008) p.143 –146.

Google Scholar

[7] C. Shao, H. Kim, J. Gong, B. Ding, D. Lee, S. Park: Mater. Lett. 57 (2003) p.1579– 1584.

Google Scholar

[8] X.H. Li, C.L. Shao, Y.C. Liu, X.T. Zhang, S.K. Hark: Mater. Lett. 62 (2008) p.2088 – (2091).

Google Scholar

[9] S. Choi, S.G. Lee, S.S. Im, S.H. Kim, Y.L. Joo: J. Mater. Sci. Lett. 22, 2003, p.891– 893.

Google Scholar

[10] K. Iimura, T. Oi, M. Suzuki, M. Hirota: Adv. Powder Technol. 21 (2010) p.64–68.

Google Scholar

[11] G. Zhang, W. Kataphinan, R. Teye-Mensah, P. Katta, L. Khatri, E.A. Evans G.G. Chase, R.D. Ramsier, D.H. Reneker: Mater. Sci. Eng., B 116 (2005) p.353–358.

DOI: 10.1016/j.mseb.2004.05.050

Google Scholar

[12] S.W. Lee, Y.U. Kim, S. Choi, Tae Y. Park Y.L. Joo, S.G. Lee: Mater. Lett. 61 (2007) p.889– 893.

Google Scholar

[13] L. Dai, X.L. Chen, T. Xhou, B.Q. Hu: J. Phys.: Condens. Matter. 14 (2002) p.473.

Google Scholar

[14] M. Andrianainarivelo, R. Corriu, D. Leclercq, P.H. Mutin, A. Vioux: J. Mater. Chem. 6 (10) (1996) p.1665.

Google Scholar