Preparation of β-PbO2 and β-PbO2-MnO2 Coating on Stainless Steel Substrate

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Abstract:

In order to prepare a new type of anode material, stainless steel was selected as substrate material. The β-PbO2 coating on stainless steel substrate was prepared under the appropriate plating solution, and the PbO2-MnO2 coating was prepared with thermal decomposition. The crystal structure was determined by X-ray diffraction; Surface morphology was test by Scanning Electron Microscopy; the energy spectrum was used to determine element mass-fraction and the ratio of atomic number of the coatings.

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Advanced Materials Research (Volumes 490-495)

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3486-3490

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March 2012

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© 2012 Trans Tech Publications Ltd. All Rights Reserved

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[1] XU Jing-fa, The development of anode material for zinc electrowinning, Nonferrous Metals (Extractive Metallurgy). 1995, 26(1): 39-41.

Google Scholar

[2] ZHOU Ya-ning, WAN Ya-zhen, LIU Jin-dun, Preparation and application of PbO2 electrode, Inorganic Chemicals Industry. 2006, 38(10): 8-11.

Google Scholar

[3] CHEN Zheng-fang, JIANG Han-ying, SHU Yu-de, et al, The effect of electrodepositing conditions of manganese dioxide and heat treatment of PbO2-Ti/MnO2 electrode on its catalytic activity and lifetime, J. Cent. South Inst Min Metal. 1991, 22 (2): 209-214.

Google Scholar

[4] YU De-long, Preparation and structure properties of MnOx electrode material, Materials Protection. 1995, 28(3): 12-14.

Google Scholar

[5] A.B. Velichenko, D.V. Girenko, F.I. Danilov, Mechanism of lead dioxide electrodeposition, Journal of Electroanalytical Chemistry. 1996, 495: 127-132.

DOI: 10.1016/0022-0728(95)04401-9

Google Scholar

[6] LI Shan-ping, HU Zhen, SUN Yi-ming, et al, Preparation and evaluation of the electro-catalytic characteristics of novel lead Ti-based dioxide electrodes, Journal of Shandong University of Technology. 2007, 37 (3): 109-113.

Google Scholar

[7] ZHANG Xiong, Controllable synthesis and property of manganese oxide and nanocomposite, Beijing University of Chemical Technology, (2008).

Google Scholar

[8] SUN Zhi-Quan LU Hai-Yan REN Xiu-Bin, et al, Performances of Ti/SnO2-Sb2O5 Anodes Prepared by Brush Coating Thermal Decomposition Method, Acta Physico-Chimica Sinica. 2009, 25(7): 1385-1390.

DOI: 10.3866/pku.whxb20090727

Google Scholar

[9] HUANG Xin-ming. Analysis methods of materials, National Defense Industry Press, Beijing, (2006).

Google Scholar