Synthesis of CaO-Na2O-Fe2O3-FeO-B2O3-SiO2 Glass-Ceramics for Hyperthermia Application by Aqueous Solution-Melt Method

Jian An Liu; Mei Mei Zhang; Xue Na Yang; Wen He

doi:10.4028/www.scientific.net/AMR.535-537.861

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HomeAdvanced Materials ResearchAdvanced Materials Research Vols. 535-537Synthesis of CaO-Na2O-Fe2O3-FeO-B2O3-SiO2...

Synthesis of CaO-Na₂O-Fe₂O₃-FeO-B₂O₃-SiO₂ Glass-Ceramics for Hyperthermia Application by Aqueous Solution-Melt Method

Abstract:

Based on the CaO-Na2O-Fe2O3-FeO-B2O3-SiO2 system, the ferrimagnetic glass-ceramic has been prepared for hyperthermia application by aqueous aolution-melt method. Using the aqueous solution solvent evaporation, we obtained the molecular-scale homogenously glass precursor. The precursor was completely melted in a lidded platinum crucible placed in an electric furnace at 1480°C for 1h and then annealed in a furnace at 550°C for 40min.The annealed glasses were heat treated at 1050°C for 2h to obtain the glass-ceramics. The crystallization of the glass systems with different component has been systematically investigated by using XRD, TG, as well as Vibrating Sample Magnetometer (VSM). The glass-ceramics with B2O3=3.0wt% show a strong magnetic, which contains highest value of specific saturation magnetization of 28.34A•m2/kg.

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Advanced Materials Research (Volumes 535-537)

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861-865

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https://doi.org/10.4028/www.scientific.net/AMR.535-537.861

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June 2012

Authors:

Jian An Liu, Mei Mei Zhang, Xue Na Yang, Wen He

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Aqueous Solution-Melt Method, Ferrimagnetic Glass-Ceramics, Magnetic Property

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