Influence of Preparation Conditions of the Solid Base Catalyst on the Performance of Synthesizing Polyglycerol

Jia Wei Qu; Min Wei Wang; Ren Lang Wang

doi:10.4028/www.scientific.net/AMR.549.109

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HomeAdvanced Materials ResearchAdvanced Materials Research Vol. 549Influence of Preparation Conditions of the Solid...

Influence of Preparation Conditions of the Solid Base Catalyst on the Performance of Synthesizing Polyglycerol

Abstract:

Different solid base catalysts used for the polymerization of glycerol were prepared by impregnation. Catalyst type and the preparation conditions were optimized on the base of polymerization degree. Results showed: the best catalyst was KF/Al₂O₃, and optimal condition for catalyst preparation was as follows: loading of 40% KF, calcinations temperature 600°C. The polymerization degree of 5.92 was obtained under the following reaction condition: the amount of catalyst 11.62,reaction temperature 250°C, reaction time 4 h.

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Periodical:

Advanced Materials Research (Volume 549)

Pages:

109-112

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.549.109

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Online since:

July 2012

Authors:

Jia Wei Qu, Min Wei Wang, Ren Lang Wang

Keywords:

Polyglycerol, Preparation Condition, Solid Base

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