The Effect of Bath Temperature on the Adhesive Strength and Bioactivity of TiO2 Nanotube Arrays

Xiu Feng Xiao; Hai Zhen Tang; Ke Guan Ouyang; Rong Fang Liu

doi:10.4028/www.scientific.net/AMR.549.724

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HomeAdvanced Materials ResearchAdvanced Materials Research Vol. 549The Effect of Bath Temperature on the Adhesive...

The Effect of Bath Temperature on the Adhesive Strength and Bioactivity of TiO₂ Nanotube Arrays

Abstract:

The effect of bath temperature on the morphologies, crystallographic structure and adhesive strength of TiO₂ nanotube arrays fabricated by electrochemical anodization of titanium in dimethyl sulfoxide containing hydrofluoric acid electrolyte were studied in this paper. The results show that the crystalline anatase TiO₂ nanotube arrays can be directly fabricated at the bath temperature above 50oC without further annealing. The crystallinity of anatase at the top of nanotubes is higher than that at the bottom of nanotubes. The bath temperature has obviously impact on the surface morphology of the titanium substrate underneath the nanotube arrays. The adhesive strength of TiO₂ nanotube arrays increases with the rise of bath temperature increasing, and reaches 11.3 MPa when TiO₂ nanotube arrays are fabricated at 60 oC.

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Periodical:

Advanced Materials Research (Volume 549)

Pages:

724-728

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.549.724

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Online since:

July 2012

Authors:

Xiu Feng Xiao, Hai Zhen Tang, Ke Guan Ouyang, Rong Fang Liu

Keywords:

Adhesive Strength, Anatase, Bath Temperature, Bioactivity, TiO₂ Nanotube Array (TNAs)

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