Optimization of Technology of Emulsion Polymerization with High Solid Content and SAS Regression Procedure

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Abstract:

A random-arranged experimental design method was employed to optimize the technology of styrene/butylacrylate/acrylic acid (St/BA/AA) emulsion polymerization with high solid content. The random-designed experimental results were analyzed with regression analysis by using statistical analysis system (SAS), and the optimal regression equations between the principal factors and the emulsion properties were in turn established. It is shown that the viscosity of emulsions is greatly affected by the following factors: solid content, the interaction between the emulsifier content and solid content, the interaction between the initiator concentration and reaction temperature, the interaction between functional monomer and reaction temperature.

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Advanced Materials Research (Volumes 554-556)

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161-167

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July 2012

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© 2012 Trans Tech Publications Ltd. All Rights Reserved

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[1] M. Schneider, J. Claverie, C. Graillat, T. F. McKenna, J. Appl. Polym. Sci. 84(2002)1878.

Google Scholar

[2] M. Schneider, J. Claverie, C. Graillat, T. F. McKenna, J. Appl. Polym. Sci. 84(2002)1897.

Google Scholar

[3] M. Schneider, J. Claverie, C. Graillat, T. F. McKenna, J. Appl. Polym. Sci. 84(2002)1916.

Google Scholar

[4] M. Schneider, J. Claverie, C. Graillat, T. F. McKenna, J. Appl. Polym. Sci. 84(2002)1935.

Google Scholar

[5] Marcelo Do Amaral, José M. Asua, J. Polym. Sci: Part A: Polym. Chem. 42(2004)4222.

Google Scholar

[6] Marcelo Do Amaral, Steven Van Es, José M. Asua, J. Polym. Sci., Part A: Polym. Chem. 42 (2004) 3936.

Google Scholar

[7] Inês de F.A. Mariz, José C. de la Cal, Jose R. Leiza, Polymer 19(2010)4044.

Google Scholar

[8] K. Ouzineb, C.Graillat, T. F. Mckenna, J. Appl. Polym. Sci. 97(2005)745.

Google Scholar

[9] Y. H. Zhang, B. Wang, M. M. Dai , S. S. Pan, F. Zhang , P. X. He, J. Macromol. Sci. Part A 48(2011)409.

Google Scholar

[10] C. Y. Zhao, J. J. Ren, Y. T. Zhang, J. S. Ma, Polym.-Plast. Technol. Eng. 50(2011)379.

Google Scholar

[11] B. Tang, J. American.Statist.Assoc. 88(1993)1392.

Google Scholar

[12] K.T. Fang, Y. Wang, Number Theoretic Methods in Statistics, Chapman and Hall, London,(1994)

Google Scholar

[13] Y. Z. Liang, K. T. Fang, Q. S. Xu, Chemometr. Intell. Lab. 58 (2001) 43.

Google Scholar

[14] X. Zh. Zhang, Math. Stat. Manag. 4(1995)43. In Chinese

Google Scholar

[15] L. P.Hu. Modem Statistics and the Application for SAS, Beijing(1996), In Chinese

Google Scholar

[16] SAS Institute Inc. SAS/STAT Guide for Personal Computers, USA(1987), In Chinese

Google Scholar

[17] D. F.HUI , practical tutorial of Statistical Analysis System SAS , Beijing(1996), In Chinese

Google Scholar