Synthesis of MoS2 Nanoparticles with Inorganic Fullerene-Like Structure from Molybdenum Trioxide and Sulfur

Bin Gao; Xiao Jun Zhang

doi:10.4028/www.scientific.net/AMR.554-556.601

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HomeAdvanced Materials ResearchAdvanced Materials Research Vols. 554-556Synthesis of MoS2 Nanoparticles with Inorganic...

Synthesis of MoS₂ Nanoparticles with Inorganic Fullerene-Like Structure from Molybdenum Trioxide and Sulfur

Abstract:

MoS₂ nanoparticles with fullerene-like (IF-MoS2) structure were successfully obtained at heating temperature higher than 840 °C by chemical vapor deposition method in a three-tube furnace using MoO₃ and S (sulfur) powders as raw materials. The synthesized samples were characterized by X-ray diffraction, field emission scanning electron microscopy, transmission electron microscopy, and energy dispersion X-ray spectrometerrespectively. IF-MoS₂ nanoparticles can be obtained only in the narrow temperature range of 840 °C-870 °C, and the diameter of IF-MoS₂ nanoparticles increases with temperature. A gradual formation mechanism of IF-MoS₂ nanoparticles was discussed in detail.

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Advanced Materials Research (Volumes 554-556)

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601-604

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https://doi.org/10.4028/www.scientific.net/AMR.554-556.601

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July 2012

Authors:

Bin Gao, Xiao Jun Zhang

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Chemical Vapor Deposition (CVD), Fullerene-Like Structure, Molybdenum Disulfide Nanoparticles

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