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HomeAdvanced Materials ResearchAdvanced Materials Research Vols. 557-559The Synthesis and Characterization of Ti-MCM-41 by...

The Synthesis and Characterization of Ti-MCM-41 by Microwave Radiation

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Abstract:

Mesoporous molecular sieve Ti-MCM-41 was synthesized by means of microwave radiation in domestic microwave oven using cetyltrimethyl ammonium bromide as template and ethyl orthosilicate, tetrabutyl titanate as raw materials, respectively. The sample is indeed Ti-MCM-41 after characterization by XRD, SEM, FT-IR and BET surface area. Compared with the reported synthesis methods, remarkable predominance of this method is that operation is simpler, crystallization time is shorter (only 40 min) and energy consumption is lower.

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Advanced Materials and Processes II

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Periodical:

Advanced Materials Research (Volumes 557-559)

Pages:

1411-1414

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.557-559.1411

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Online since:

July 2012

Authors:

Juan Zhang, Di Shun Zhao, Meng Shuai Liu, Jun Pan Li

Keywords:

Domestic Microwave Oven, Microwave Radiation, Synthesis, Ti-MCM-41

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© 2012 Trans Tech Publications Ltd. All Rights Reserved

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