Preparation of ZnAl2O4 Spinel Directly from Zinc Aluminum Layered Double Hydroxide Precursor

Article Preview

Abstract:

Single-phase ZnAl2O4 spinel has been prepared by a novel simple route using layered double hydroxide as a precursor. ZnAl2O4 spinel is directly obtained by calcination of zinc aluminum layered double hydroxide (Zn/Al molar radio is 0.5) without further chemical treatment. The key feature of this method is that it affords uniform distribution of all metal cations on an atomic level in the precursor. The structural characteristics of the as-synthesized precursor and the resulted calcined products are obtained by X-ray diffraction and scanning electron microscope.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

127-130

Citation:

Online since:

September 2012

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2012 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

[1] F. Cavani, F. Trifirò and A. Vaccar: Catal Today vol. 11 (1991), p.173.

Google Scholar

[2] A.M. Fogg, G.R. Williams, R. Chester, et al: J. Mater. Chem vol. 14 (2004), p.2369.

Google Scholar

[3] R. Chitrakar, Y. Makita, A. Sonoda, et al: J. Hazard. Mater vol. 185 (2011), p.1435.

Google Scholar

[4] Z. P. Xu, J. Zhang and O.A. Moses: Appl Clay Sci vol. 53 (2011), p.139.

Google Scholar

[5] E. Han, D. Shan and H. G. Xue: Biomacromolecules vol. 8 (2007), p.971.

Google Scholar

[6] M. R. Berber, I. H. Hafez, K. Minagawa, et al: Pharm Res vol. 27 (2010), p.2394.

Google Scholar

[7] F. Li, J. J. Liu, G. David, et al: Chem. Mater vol. 16 (2004), p.1597.

Google Scholar

[8] W. Kanjina and W. Trakarnpruk: Chin. Chem. Lett vol. 22 (2011), p.401.

Google Scholar

[9] W. Walerczyk, M. Zawadzki and J. Okal: Appl. Surf. Sci vol. 257 (2011), p.2394.

Google Scholar

[10] G. Lakshminarayana and L. Wondraczek: J. Solid. State. Chem vol. 184 (2011), p. (1931).

Google Scholar

[11] S. K. Sampath, D. G. Kandive and R. Pandey: J. Physics: Condensed Matter vol. 11 (1999), p.3635.

Google Scholar

[12] L. Zou, F. Li, X. Xiang, et al: Chem. Mater vol. 18 (2006), p.5852.

Google Scholar

[13] X. J. Wang, M. C. Zhang, H. Ding, et al: J. Alloys. Compd vol. 509 (2011), p.6317.

Google Scholar

[14] Mu. T. Tsai, Y. X. Chen, P. J. Tsai, et al: Thin. Solid. Films vol. 518 (2010), p. e9.

Google Scholar