Optimization on Influencing Factors of Fracture Toughness of Corundum-Mullite Toughened by In Situ Synthesized Mullite Whiskers by Response Surface Methodology

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Abstract:

The corundum-mullite was toughened by in-situ synthesized mullite whiskers and the process parameters influencing the fracture toughness of corundum-mullite, such as sintering temperature, addition amount of AlF3 and V2O5, were optimized by means of response surface method. Corundum-mullite with fracture toughness of 9.44 MPa.m-1/2 could be obtained under the optimized conditions, i.e. sintering temperature of 1400°C, 4.8 wt.% of AlF3 and 5.8 wt.% of V2O5. The results showed that it was feasible to prepare corundum-mullite toughened by in-situ synthesized mullite whiskers by the optimized parameters. In addition, an accurate model based on response surface method was proposed to predict the experimental results.

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Advanced Materials Research (Volumes 581-582)

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819-822

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October 2012

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© 2012 Trans Tech Publications Ltd. All Rights Reserved

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