Effects of Preparation Conditions on Characters of Hydrophobic Silica Granular Aerogel and its Applications

Article Preview

Abstract:

The hydrophobic silica granular aerogels were synthesized via sol-gel synthesis followed by ambient pressure drying. The tetraethyloxylane (TEOS) was used as original precursor. The aerogels were analyzed using nitrogen adsorption, scanning electron microscopy (SEM) and laser particle size analyzer. It was found that the aerogel was mesoporous material with high surface area. The aerogels were prepared in grain form by dipping into disperse solution in order to adsorption application. The average particle size of the aerogel was controlled by pH and disperse solution volume. The pH also affected gel time. The aerogels were used to absorb phenol from water. The saturated adsorption amount could reach up to 145 mg•g-1.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

190-193

Citation:

Online since:

November 2012

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2012 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

[1] Soleimani Dorcheh, M.H. Abbasi. Silica aerogel; synthesis, properties and characterization. Journal of materials processing technology 199 (2008) 10–26.

DOI: 10.1016/j.jmatprotec.2007.10.060

Google Scholar

[2] L. W. Hrubesh, P. R. Coronado, J. H. Satcher Jr. Solvent removal from water with hydrophobic aerogels. Journal of Non-Crystalline-Crystalline Solids 285 (2001) 328–332.

DOI: 10.1016/s0022-3093(01)00475-6

Google Scholar

[3] A. Venkateswara Rao, Nagaraja D. Hegde, Hiroshi Hirashima. Absorption and desorption of organic liquids in elastic superhydrophobic silica aerogels. Journal of Colloid and Interface Science 305 (2007) 124–132.

DOI: 10.1016/j.jcis.2006.09.025

Google Scholar

[4] A. Parvathy Rao, A. Venkateswara Rao , G.M. Pajonk. Hydrophobic and physical properties of the ambient pressure dried silica aerogels with sodium silicate precursor usingvarious surface modification agents. Applied Surface Science 253 (2007).

DOI: 10.1016/j.apsusc.2006.12.117

Google Scholar

[5] A. Venkateswara Rao , Sharad D. Bhagat , Hiroshi Hirashima , G.M. Pajonk. Synthesis of flexible silica aerogels using methyltrimethoxysilane (MTMS) precursor. Journal of Colloid and Interface Science 300 (2006) 279–285.

DOI: 10.1016/j.jcis.2006.03.044

Google Scholar

[6] Suzana Štandeker, Zoran Novak, Željko Knez. Adsorption of toxic organic compounds from water with hydrophobic silica aerogels. Journal of Colloid and Interface Science 310 (2007) 362–368.

DOI: 10.1016/j.jcis.2007.02.021

Google Scholar