Sn-Ni Nano Particle Prepared by a Chemical Reduction Method

Article Preview

Abstract:

Sn-Ni intermetallic compounds have been prepared by a chemical reduction method. With different molar ratios of Sn/Ni, the products are different. XRD determination results indicate that the main phases of the products with Sn/Ni=1:0.5 and 1:1.0 are Sn6O4(OH)4 and metal Sn, and the main phases of the products with Sn/Ni=1:1.5 and 1:2.0 are SnNi, Ni3Sn and metal Sn. SEM investigation finds that the particle size of the products with Sn/Ni=1:1.5 and 1:2.0 are nano size, and the particle size increases with increasing Ni content. The particles of the product with Sn/Ni=1:1.5 are in the range of 50-100nm, and well dispersed.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

259-262

Citation:

Online since:

December 2012

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2013 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

[1] J.M. Tarascon, M. Armand: Nature Vol. 414(2001), p.359.

Google Scholar

[2] M. Winter, J.O. Besenhard, M.E. Spahr, et al: Adv. Mater. Vol. 10(1998), p.725.

Google Scholar

[3] I.A. Courtney, J.R. Dahn: J. Electrochem. Soc. Vol. 144(1997), p. (2045).

Google Scholar

[4] S.D. Beattie, J.R. Dahn: J. Electrochem. Soc. Vol. 150(2003), p. A894.

Google Scholar

[5] G.M. Ehrlich, C. Durand, X. Chen, et al: J. Electrochem. Soc. Vol. 147(2000), p.886.

Google Scholar

[6] O. Mao, J.R. Dahn: J. Electrochem. Soc. Vol. 146(1999), p.414.

Google Scholar

[7] M. Winter, J.O. Besenhard, Electrochim. Acta Vol. 45 (1999), p.31.

Google Scholar

[8] J. Hassoun, S. Panero, P. Simon, et al: Adv. Mater. Vol. 19(2007), p.1632.

Google Scholar

[9] I. Amadei, S. Panero, B. Scrosati, et al: J. Power Sources Vol. 143( 2005), p.227.

Google Scholar

[10] A. Aricò, P. Bruce, B. Scrosati, et al: Nat. Mater. Vol. 4(2005), p.366.

Google Scholar

[11] H.C. Shin, M. liu: Adv. Funct. Mater. Vol. 15(2005), p.582.

Google Scholar