Hydrothermal Synthesis of Analcime from Local Pottery Stone

Amnouy Larpkasemsuk; Saowaroj Chuayjuljit; Wirapong Kornpanom; Dujreutai Pongkao Kashima

doi:10.4028/www.scientific.net/AMR.664.801

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HomeAdvanced Materials ResearchAdvanced Materials Research Vol. 664Hydrothermal Synthesis of Analcime from Local...

Hydrothermal Synthesis of Analcime from Local Pottery Stone

Abstract:

In this study, local pottery stone (PTS) was hydrothermal treated with 2 M of NaOH at different reaction temperatures (60, 80 and 120°C) and times (8, 12 and 24 h) in a Teflon-lined stainless steel autoclave in order to synthesize analcime fine powders. All the as-prepared samples were characterized for their phase composition and morphology using X-ray diffraction (XRD) and scanning electron microscopy (SEM), respectively. The results showed that under the conditions investigated, pure analcime could be obtained only at 120°C for all synthesis durations. The analcime microcrystalline particles exhibit isometric trapezohedron or deltoidal icositetrahedron morphology with narrow size distribution from 8 to 14 µm.

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Periodical:

Advanced Materials Research (Volume 664)

Pages:

801-805

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.664.801

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Online since:

February 2013

Authors:

Amnouy Larpkasemsuk, Saowaroj Chuayjuljit, Wirapong Kornpanom, Dujreutai Pongkao Kashima

Keywords:

Analcime, Hydrothermal Method, Morpholoy, Phase Composition, Pottery Stone

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