Effect of Sintering Time and Heating Rate on the Structure of LiFePO4/C Prepared by Electrospinning

Chang Huan Zhang; Yin Zheng  Liang; Yi Ping  Qiu

doi:10.4028/www.scientific.net/AMR.760-762.797

Paper Titles

Experimental Study of Low-Pressure Water Jet Assisted Laser Drilling on Al₂O₃ Ceramic
p.780

New Type Intellectualized Clothing Materials-Color-Changing Materials
p.785

Synthesis of Nickel Nanoparticles/Multiwalled Carbon Nanotubes Composites with Pre-Treated Multiwalled Carbon Nanotubes as Modifier
p.789

Synthesis of Graphene Load Nickel Nanoparticles Composites with Hydrothermal Process
p.793

Effect of Sintering Time and Heating Rate on the Structure of LiFePO₄/C Prepared by Electrospinning
p.797

Local Electric Field Enhancement of Neighboring Ag Nanoparticles in Surface Enhanced Raman Scattering
p.801

The Optimization and Experiment of the Low-Pressure Water Jet Assisted Laser Etching on Al₂O₃ Ceramic
p.806

Synthesis, Crystal Growth and Characterization of Organic Nonlinear Optical Co-Crystal: 4-N, N-dimethylamino-4-N-methyl-stilbazolium (3-nitrobenzenesulfonate)_0.6I_0.4
p.811

Effect of Growth Conditions on Morphology and Photoluminescence Properties of ZnO Nanowires Fabricated by Thermal Evaporation without a Metal Catalyst
p.816

HomeAdvanced Materials ResearchAdvanced Materials Research Vols. 760-762Effect of Sintering Time and Heating Rate on the...

Effect of Sintering Time and Heating Rate on the Structure of LiFePO₄/C Prepared by Electrospinning

Abstract:

The electrospinning combined with the sintering process were used to prepare carbon-coated lithium iron phosphates (LiFePO₄/C) cathode materials for lithium ion batteries (LIB). In sintering process, different procedures were used to synthesize the LiFePO₄/C composite materials. The effect of the sintering time and heating rate on the structure, surface morphology and carbon content of LiFePO₄/C composite materials were investigated by wide angel X-ray diffraction (WXRD), scanning electron microscope (SEM), and elemental analysis (EA) techniques. It has better structure when the sintering process is as follows: heating rate is 2 oC min^-1 and pre-oxidized time is 3h at 280 oC and carbonized time is 8h at 700 oC.

You might also be interested in these eBooks

View Preview

Info:

Periodical:

Advanced Materials Research (Volumes 760-762)

Pages:

797-800

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.760-762.797

Citation:

Cite this paper

Online since:

September 2013

Authors:

Chang Huan Zhang, Yin Zheng Liang, Yi Ping Qiu

Keywords:

Electro-Spinning, Heating Rate, Lithium Iron Phosphates (LiFePO₄), Sintering Time

Export:

RIS, BibTeX

Price:

Permissions CCC:

Request Permissions

Permissions PLS:

Request Permissions

Сopyright:

Citation:

References

[1] J. M. Tarascon, M. Armand: Nature Vol. 414 (2001), pp.359-367.

Google Scholar

[2] Shinichi Nishimura, Genki Kobayashi, Kenji Ohoyama, et al: Nature Materials Vol. 7 (2008) , pp.707-711.

Google Scholar

[3] A. K. Padhi, K. S. Nanjundaswamy, J. B. Goodenough: Journal of the Electrochemical Society Vol. 144(4) (1997), pp.1188-1194.

Google Scholar

[4] Franger, S., Le Cras, F., Bourbon, C., et al: J. Electrochem. Soc. Vol. 26 (2004), p. A1024-A1027.

Google Scholar

[5] Franger, S., Bourbon, C., Le Cras, F.: J. Power Sources Vol. 119 (2003), pp.252-257.

Google Scholar

[6] N. N. Sinha, C. Shivakumara, N. Munichandraiah: ACS Applied Materials & Interfaces Vol. 2, No. 7 (2010), p.2031-(2038).

Google Scholar

[7] Jiajun Wang, Xueliang Sun: Energy & Environmental Science Vol. 5 (2012), pp.5163-5185.

Google Scholar

[8] Hao Hsun Chang, Chun Chih Chang, Hung Chun Wu, et al: Journal of Power Sources Vol. 158 (2006), pp.550-556.

Google Scholar