Effect of Annealing Temperature on TiO2 Nanostructured Prepared by Sol-Gel Method

S.K.M. Maarof; Mohamad Rusop; Saifollah Abdullah

doi:10.4028/www.scientific.net/AMR.832.763

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HomeAdvanced Materials ResearchAdvanced Materials Research Vol. 832Effect of Annealing Temperature on TiO2...

Effect of Annealing Temperature on TiO₂ Nanostructured Prepared by Sol-Gel Method

Abstract:

Titanium Dioxide, TiO₂ is one of the potential semiconductor materials. TiO₂ has much application such as for pigments, oxygen sensors, and photocatalyst. Recently, the researcher study on the other application and revealed that this material has a great potential to be use in nanocoating area. The objective of this paper is to produce TiO₂ nanostructured prepared by sol-gel method. Sol-gel was carried out using tetra (IV) isopropoxide (TTIP), absolute ethanol, Acetic Acid Glacial (GAA), Triton-X-100 and deionized water and all the solution was mixing by continuous stirring and heating. After finished prepare the sol-gel, solution will be spin coated onto glass substrate and annealed with different temperature for 2 hours. The particles were analyzed using Raman Spectroscopy to observe the crystallographic phase, and the morphology was evaluated through Atomic Force Microscopy (AFM). As a result, TiO₂ that annealed at 450°C shows the better nanostructured compared to other annealing temperature. Keywords: Titanium Dioxide (TiO₂); Sol-gel method ; Spin-coating ; Annealing process ; Raman spectroscopy

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Periodical:

Advanced Materials Research (Volume 832)

Pages:

763-766

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.832.763

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Online since:

November 2013

Authors:

S.K.M. Maarof, Mohamad Rusop, Saifollah Abdullah

Keywords:

Annealing Process, Raman Spectroscopy, Sol-Gel Method, Spin-Coating, Titanium Dioxide (TiO₂)

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References

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DOI: 10.4028/www.scientific.net/amr.364.12

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