Grain Refinement Mechanism of MgAlON Composites Prepared by Spark Plasma Sintering

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The paper developed a computing model to analyze the grain refinement mechanism of MgAlON composites sintered by spark plasma sintering (SPS). Using alumina, magnesia and aluminum as raw materials MgAlON composites were prepared by SPS. Based on the current assignment principle, the heating rate at different positions in Al grains was analyzed, and the particle radius during the sintering process could be calculated. The results suggested that necks could be formed between MgAlON particles with electric current heating rapidly to reduce particle radius, the shorter vertical distance from the interface was, the larger heating rate and growing rate of the neck had; the necks between particles be formed dynamically in the sintering process, so the big particle radius would be getting smaller and smaller continually so that we could get a large amount of micro particles distributed uniformly in the sintered MgAlON composites, and the resulted grain refinement was more obvious.

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115-119

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November 2013

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© 2014 Trans Tech Publications Ltd. All Rights Reserved

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[1] Wang Xiufen, Zhou Xiya, Spark plasma sintering technology, China Ceramics. 42(7) (2006) 14-16.

Google Scholar

[2] Zhang Houxing, Huang Yong, Li Haifeng, Study on the superfast synthesis of MgAlON spinel by spark plasma sintering (SPS), Journal of Ceramics. 26(1) (2005) 13-16.

Google Scholar

[3] Yuan Huiyu: Study on Preparation and Thermal Stability of Microcrystalline MgAlON and Corundum Composites, Zhengzhou University, China, (2011).

Google Scholar

[4] Xiaoyan Song, Xuemei Liu, Jiuxing Zhang, Neck formation and self-adjusting mechanism of neck growth of conducting powders in spark plasma sintering, J Am Ceram Soc. 89(2) (2006) 494-500.

DOI: 10.1111/j.1551-2916.2005.00777.x

Google Scholar

[5] Liu Xuemei, Song Xiaoyan, Zhang Jiuxing, Study on mechanism of homogenous neck growth of conductive pure materials during SPS, in: Junyou Liu (Eds. ), Academic Proceedings Presented in the 7th China Material Science and Image Technology Conference, Chinese Society for Stereology, Beijing, 2009, pp.128-134.

Google Scholar