The Synthesis of a Polyaspartic Acid Ester and Development of the Coatings

Xiao Ping Liu; Tian Liang Zheng

doi:10.4028/www.scientific.net/AMR.842.297

Paper Titles

Grain Refinement of Mg₉₇Y₂Cu₁ Alloy Solidified with Pulsed Direct Current Magnetic Field
p.279

Springback Experimental Research of Advanced High-Strength Steel
p.284

Direct Synthesis and Characterization of Three-Dimensional Graphene Foam
p.289

Nd,Yb:YAG Laser Crystal Production and its Property
p.293

The Synthesis of a Polyaspartic Acid Ester and Development of the Coatings
p.297

Effect of Interlayers on the Structure and Properties of TiAlSiN Coatings Deposited on High-Speed Steel Substrate
p.302

An Investigation of Carburized Layers on Austenitic Stainless Steels
p.307

Effect of Cold Spray Processes on Friction Stir Welded Microstructures of AZ31 Magnesium Alloys
p.311

Ceramic Powder (Silicon Carbide) - Monitoring and Influencing Process its Production
p.316

HomeAdvanced Materials ResearchAdvanced Materials Research Vol. 842The Synthesis of a Polyaspartic Acid Ester and...

The Synthesis of a Polyaspartic Acid Ester and Development of the Coatings

Abstract:

A new type of polyaspartic acid ester (PAE) was synthesized by double alkyl malay acid ester and bis-(p-aminocyclohexy) methane (PACM) via a Michael addition reaction. The Fourier transform infrared spectrometer shows the reaction can take place in room temperature. The dynamics of the reaction were investigated by mercaptan-iodine titration analysis method at 57°C and 67°C. The results showed the reaction order between double alkyl malay acid ester and bis-(p-aminocyclohexy) methane (PACM) was three. The solvent free polyaspartic polyurea coating was developed with the synthesized resin and the properties were tested with good results.

You might also be interested in these eBooks

Materials, Mechanical and Manufacturing Engineering

View Preview

Info:

Periodical:

Advanced Materials Research (Volume 842)

Pages:

297-301

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.842.297

Citation:

Cite this paper

Online since:

November 2013

Authors:

Xiao Ping Liu, Tian Liang Zheng

Keywords:

Dynamic, Polyaspartic Acid Ester, Polyurea Coatings

Export:

RIS, BibTeX

Price:

Permissions CCC:

Request Permissions

Permissions PLS:

Request Permissions

Сopyright:

Citation:

References

[1] HUANG Wei-bo. Polyurea elastomer technology [M]. Beijing: chemical industry press, 2005, 5.

Google Scholar

[2] Douglas A Wicks, Philip E Yeake. Amine chemistries for isocyanate based coating [J]. Progress in organic coatings, 1997, 30(4): 165~270.

DOI: 10.1016/s0300-9440(97)00002-7

Google Scholar

[3] D.K. Chattopadhyay, K.V.S.N. Raju. Structural engineering of polyurethane coatings for high performance applications [J]. Progress in polymer science, 2007, (32): 352~418.

DOI: 10.1016/j.progpolymsci.2006.05.003

Google Scholar

[4] Alejandro Sosnik, Gustavo Gotelli, Gustavo A. Abraham. Microwave-assisted polymer synthesis as a tool in biomaterials since: How new and how powerful [J]. Progress in polymer science, 2011, (36): 1050~1078.

DOI: 10.1016/j.progpolymsci.2010.12.001

Google Scholar

[5] Lv Ping, CHEN Guo-ping, HUANG Wei-bo. Aliphatic polyurea coating based on novel polyaspartic ester [J]. Polymer materials science and engineering, 2007, (25): 55~58.

Google Scholar

[6] CHEN Guo-ping, LV Ping, HUANG Wei-bo. Novel aliphatic polyurea elastomer based on polyaspartic ester [J]. Periodical of ocean university of China, 2008, (38): 315~318.

Google Scholar

[7] LIU Pei-li, LIU Guang-ye, HUANG Wei-bo. Preparation and study of polyaspartic polyurea [J]. Polyurethane industry, 2005, (20): 16~19.

Google Scholar

[8] HUANG Wei-bo, LIU Pei-li, HU Song-xia, LU Ming. Polyaspartic, new material of spraying polyurea technology field [J]. China paint, 2005, (20): 36~38.

Google Scholar

[9] XUE Shou-cheng, XI Fa-chen, FENG Jun-zhong, CHEN Xiao-qing, LI Qing-cai, WANG Guo-wei. Synthsis and application of new polyaspartic ester in elastic polyurethane coatings [J]. Modern paint & finishing, 2009, (12): 1~4.

Google Scholar

[10] Lv Ping, CHEN Guo-ping, HUANG Wei-bo. Structure and properties of novel polyurea based on polyaspartic ester [J]. China synthetic rubber industry, 2007, (4): 263~266.

Google Scholar