Analysis of the Rheological Behavior and Stability of Inconel 718 Powder Injection Molding (PIM) Feedstock

Article Preview

Abstract:

In PIM process, the molding stage is a critical step for the fabrication of sound parts without cracks and distortions. So, this step requires specific rheological behavior. Rheological analysis can be made to quantify the stability of the PIM feedstock during molding process. In this study, an experimental rheological study has been performed to evaluate the influence of palm stearin on the rheological behavior and stability of Inconel 718 powder injection molding (PIM) feedstock. The effects of shear rate and temperature were investigated via capillary rheometer method. The viscosity and shear rate of the feedstock were measured at various range of temperature and shear rate across the L/D = 1 capillary rheometer. The results show that the formulation binder system PSPE 7030 is the best feedstock to be injection molded because it has moderate value of flow sensitivity index, lower value for flow activation energy and higher value for mold ability index. Besides that, the increasing of PS content in the binder system has found reduce viscosity and value of flow activation energy and increase value of mold ability index of feedstock.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

63-72

Citation:

Online since:

January 2014

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2014 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

[1] German R.M. & Bose A., Injection Moulding of Metals and Ceramics. Metal Powder Industries Federation. (1997) 3-10.

Google Scholar

[2] Merhar J.R., Overview of Metal Injection Moulding'. Metal Powder Report; 45(5) (1990) pp.339-342.

DOI: 10.1016/s0026-0657(10)80242-5

Google Scholar

[3] Liu Z.Y., Loh N.H., S.B. Tor and K. A. Khor, Characterization of Powder Injection Moulding Feedstock, Material Characterization 49 (2003) pp.313-320.

DOI: 10.1016/s1044-5803(02)00282-6

Google Scholar

[4] Chung C.I & Rhee B.O., Requirements of binder for powder injection moulding,. Compending Metal Injection Moulding, vol 2 (5) (1987) pp.269-77.

Google Scholar

[5] C. Mutsuddy & R. G. Ford, Ceramics Injection Moulding, Champion Hall, London (1995).

Google Scholar

[6] R. M. German, A. Bose, Injection Moulding of Metals and Ceramics, MPIF, Princeton, New Jersey, 1997.

Google Scholar

[7] Dihoru, L.V., Smith, L.N., and German, R.M. , Experimental analysis and neural network modelling of the rheological behaviour of powder injection moulding feedstock formed with bimodal powder mixtures, Powder Metallurgy, Volume 43 No.1, (2000) pp.31-36.

DOI: 10.1179/pom.2000.43.1.31

Google Scholar

[8] M. Khakbiz, A. Simchi, R. Bagheri, Analysis of the rheological behavior and stability of 316L stainless steel-TiC powder injection molding feedstock,. Materials Science and Engineering A 407. (2005) pp.105-113.

DOI: 10.1016/j.msea.2005.06.057

Google Scholar

[9] Huang,B., Liang,S., and Qu, X., The rheology of metal injection molding, Journal of Materials Processing technology, Vol.1237 (2003) pp.132-137.

DOI: 10.1016/s0924-0136(02)01100-7

Google Scholar

[10] Karatas, C., Kocer, A., Unal, H.I., and Saritas, S., Rheological properties of feedstock prepared with steatite powder and polyethylene-based thermoplastic binders", Journal of Materials Processing Technology, Vol 152 (2004) pp.77-83.

DOI: 10.1016/j.jmatprotec.2004.03.009

Google Scholar

[11] Ismail., Omar M.A., Subuki,I.,Abdullah, N., Ali, E.A.G.E., & Hassan, N., Characterization of the feedstock for metal injection molding using biopolymer binder , Reg. Conf. On Eng.Math, Mech., Manu. & Arch (EMARC) (2007) pp, 85-92.

Google Scholar

[12] Mohd Afian Omar, The influence of stearic acid on the properties of injection molding of stainless steel powder, Journal of Technology, Vol.10, No.2 (2001) pp.37-45

Google Scholar

[13] Sri Yulis M.Amin, Khairul Rijal Jamaludin & Norhamidi Muhamad , Rheological properties of SS316L MIM feedstock prepared with different particle sizes and powder loadings , Journal- The Institution of engineering, Malaysia, vol.71, No.2. (2009) pp.59-63.

Google Scholar

[14] Tseng, W.J., Liu, D.-M., Hsu, C.-K., Influence of Stearic Acid on Suspension Structure and Green Microstructure of Injection Molded Zirconia Ceramics, Ceramic International 25, 1999, pp.191-195.

DOI: 10.1016/s0272-8842(98)00024-8

Google Scholar

[15] Iriany, Rheology properties study on the feedstock contains palm stearin for metal injection molding, Doctor of Philosophy Thesis, National University of Malaysia (2002).

Google Scholar

[16] Mohd Afian Omar, Istiqamah Subuki, Norsyakirah & Mohd Fashies Ismail, The Influence of Palm Stearin Content on The Rheological Behavior of 316L Stainless Steel MIM compacts, Journal of Science and Technology, Vol 2, No 2 (2010) pp.1-14.

Google Scholar

[17] Tseng, W. J., Liu, D.M., Hsu, C.K, Influence of stearic acid on suspension structure and green microstructure of injection molded zirconia ceramics, Ceramic International 25 (1999) pp.191-195

DOI: 10.1016/s0272-8842(98)00024-8

Google Scholar

[18] Li Yimin, Qu Xuanhui, Huang Baiyun, Qiu Guanghan, Rheological properties of metal injection molding binder and feedstock, Trans. Nonferrous Met. Soc. China, Vol.7 No.3 Sept.(1997)

Google Scholar

[19] Sri Yulis, M.Amin, Khairul Rijal Jamaludin and Norhamidi Muhamad, Rheological Properties of SS316L MIM feedstock prepared with different particle sizes and powder loadings, Journal- The Institution of Engineers, Malaysia (Vol.71,No.2,June 2009)

Google Scholar

[20] Hooman Abolhasani, Norhamidi Muhamad, Rheological Investigation of A starch-based binder and feedstock for metal injection molding, International Journal of Mechanical and Materials Engineering (IJMME), vol.4, No.3(2009) pp.294-299

Google Scholar