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Synthesis of Loaded Silver 4A Zeolite Molecular Sieve with Magnetic Cores of SiO2/(γ-Fe2O3- SiO2) for Demercuration
Abstract:
It is an effective solution to the problem of agglomeration using the magnetic composite SiO2/(γ-Fe2O3- SiO2) instead of traditional magnetic particles Fe3O4 as the core of molecular sieve. The traditional hydrothermal method was utilized by means of adding the magnetic composite particles SiO2/(γ-Fe2O3- SiO2) into the pre-made crystallization liquid. Then, a series of magnetic 4A zeolites with varying contents of SiO2/(γ-Fe2O3- SiO2) were synthesized under the condition of ultrasonic crystallization for 6 hours with the power of 100W and temperature of 70 °C . Afterwards, the characterization tests such as XRD,SEM,TG,IR were carried out; the final result showed that the performance of 4A zeolite molecular sieve with SiO2/(γ-Fe2O3- SiO2) is basically identical with the pure 4A zeolite molecular sieve. The absorption rate was 13.5927μg/g by using the 4A zeolite molecular sieve with SiO2/(γ-Fe2O3- SiO2) for the absorption of mercury. Key words: 4A zeolite molecular sieve; magnetic composite; silver loaded;Demercuration
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1144-1148
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January 2014
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© 2014 Trans Tech Publications Ltd. All Rights Reserved
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