Effect of Temperature on the Purity, Particle Size and Morphology of Fe2O3 Nanomaterials

Abdul Rahman Noor Azreen; Norlida Kamarulzaman; Nurhanna Badar; Mustaffa Nur Amalina; Kamarudin Norashikin

doi:10.4028/www.scientific.net/AMR.895.305

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HomeAdvanced Materials ResearchAdvanced Materials Research Vol. 895Effect of Temperature on the Purity, Particle Size...

Effect of Temperature on the Purity, Particle Size and Morphology of Fe₂O₃Nanomaterials

Abstract:

Iron Oxide, Fe₂O₃, has extensively been studied by many researchers because of their important uses for various applications such as magnetic storages, catalysts, anode, gas sensors and biomedical applications. In our work, Fe₂O₃have been synthesized via a new self-propagating combustion (SPC) route using a weak organic acid as an oxidant. The precursor was annealed at three different temperatures. Three samples of Fe₂O₃heated at 300 °C, 600 °C and 800 °C for 24 hours were characterized using X-Ray Diffraction (XRD) and Field Emission Scanning Electron Microscopy (FESEM). The XRD pattern confirms that the crystal structure for both 600 °C and 800 °C samples are rhombohedral while for the 300 °C sample, rhombohedral and cubic phases are present. The SEM images showed that the 300 °C and 600 °C materials have irregular shapes. For the 800 °C sample the materials seem to be more crystalline with individual polyhedral shapes.

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Advanced Materials Research (Volume 895)

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305-308

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https://doi.org/10.4028/www.scientific.net/AMR.895.305

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Online since:

February 2014

Authors:

Abdul Rahman Noor Azreen*, Norlida Kamarulzaman, Nurhanna Badar, Mustaffa Nur Amalina, Kamarudin Norashikin

Keywords:

Annealing, Nanomaterial, Ron Oxide

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References

[1] M. Mohapatra, S. Anand, Int. J. Eng. Sci. Tech. 2 (2010) 127-146.

Google Scholar

[2] A.K. Gupta, M. Gupta, Biomaterials 26 (2005) 3995-4021.

Google Scholar

[3] A. Mao, J.K. Kim, K. Shin, D.H. Wang, P.J. Yoo, G.Y. Han, J.H. Park, J. Power Sources 210 (2012) 32-37.

Google Scholar

[4] H. Liu, G. Wang, J. Park, J. Wang, H. Liu, C. Zhang, Electrochim. Acta 54 (2009) 1733-1736.

Google Scholar

[5] A. Prakash, A.V. McCormick, M.R. Zachariah, Chem. Mater. 16 (2004) 1466-1471.

Google Scholar

[6] D. Peng, S. Beysen, Q. Li, Y. Sun, L. Yang, Particuology 8 (2010) 386-389.

Google Scholar

[7] X. Liao, J. Zhu, W. Zhong, H-Y. Chen, Mater. Letters 50 (2001) 341-346.

Google Scholar

[8] M.F.R. Fouda, M.B. El-Kholy, S.A. Moustafa, A.I. Hussien, M.A. Wahba, and M.F. El-Shahat: submitted to International Journal of Inorganic Chemistry (2010).

Google Scholar

[9] D. Chen, X. Jiao, D. Chen, Mater. Res. Bull. 36 (2001) 1057-1064.

Google Scholar

[10] Y.Y. Fu, R.M. Wang, J. Xu, J. Chen, Y. Yan, A.V. Narlikar, H. Zhang, Chem. Phys. Lett. 379 (2003) 373-379.

Google Scholar

[11] K. Xie, J. Li, Y. Lai, W. Lu, Z. Zhang, Y. Liu, L. Zhou, H. Huang, Electrochem. Commun. 13 (2011) 657-660.

Google Scholar

[12] P. Dhiman, A. Kumar, M. Singh, Adv. Mat. Lett. 3 (2012) 330-333.

Google Scholar

[13] A. Qurashi, Z. Zhong, M.W. Alam, Solid State Sci. 12 (2010) 1516-1519.

Google Scholar

[14] N. Kamarulzaman, R.H.Y. Subban, K. Ismail, N. Othman, W.J. Basirun, M.A. Bustam, S.A. Fuad, R. Yusof, A.F. Fadzil, Ionics 11 (2005) 446-450.

DOI: 10.1007/bf02430264

Google Scholar