Nanoemulsion Synthesis of Magnetic-Optical CoNiAu Nanoparticles

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Abstract:

Multi-functional CoNiAu nanoparticles were successfully synthesized via nanoemulsion method with the use of PEO-PPO-PEO as the surfactant, C14H29CH(OH)CH2OH as the reducing agent, Ni (acac)2, Co (acac)2 and Au (ac)3 as precursors. The characterization of the CoNiAu nanoparticles was performed using X-ray powder diffraction (XRD), fourier transform infrared spectroscopy (FTIR), transmission electron microscopy (TEM), vibrating sample magnetometry (VSM) and UV-vis near IR spectrophotometer (UV-vis). The XRD and TEM analysis confirm the formation and structure of the nanoparticles. The UV-vis and VSM measurements display the optical and magnetic properties of the CoNiAu nanoparticles at the room temperature. The CoNiAu nanoparticles with the well defined optical and magnetic properties are promised for optical, magnetic, catalytic and biomedical applications.

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90-94

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March 2014

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© 2014 Trans Tech Publications Ltd. All Rights Reserved

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[1] D. Ling, K. Domen, K. Tanaka, Electrodeposited Au-Fe, Au-Ni and Au-Co alloy nanoparticles from aques electrolytes, Langmuir. 18 (2002) 3226-3232.

DOI: 10.1021/la010715v

Google Scholar

[2] H. Johll, H. C. Kang, Density functional theory study of Fe, Co and Ni adatoms and dimmers adsorbed on grapheme, Phys. Rev. 245416 (2009) 1-18.

DOI: 10.1103/physrevb.79.245416

Google Scholar

[3] Q.Y. Liu, X.H. Guo, T.J. Wang, Synthesis of CoNi nanowires by heterogeneous nucleation in polyol, Mater. Lett. 64 (2010) 1271-1274.

DOI: 10.1016/j.matlet.2010.03.006

Google Scholar

[4] W.H. Lu, D.B. Sun, H.Y. Yu, Synthesis and magnetic properties of size-controlled CoNi alloy nanoparticles, J. Alloys. Compd. 546 (2013) 229-233.

DOI: 10.1016/j.jallcom.2012.08.063

Google Scholar

[5] J.F. Bondi, R. Misra, X.L. Ke, Optimized Synthesis and Magnetic Properties of Intermetallic Au3Fe1-x, Au3Co1-x, and Au3Ni1-x Nanoparticles, Chem. Mater. 22 (2010) 3988-3994.

Google Scholar

[6] H.L. Liu, W.X. Zhang, Facile growth of monocrystalline gold-iron nanocrystals by polymer nanoemulsion, Gold. Bull. 44 (2011) 21-25.

DOI: 10.1007/s13404-010-0003-4

Google Scholar

[7] M.A. Garcia, P. Crespo, Surface plasmon resonance of capped Au nanoparticles, Phys. Rev. 241403 (2005) 1-4.

Google Scholar

[8] Y. C. Yeh, B. Creran, V.M. Rotello, Gold nanoparticles: preparation, properties, and applications in bio-nanotechnology, Nanoscale. 4 (2012) 1817-1880.

DOI: 10.1039/c1nr11188d

Google Scholar

[9] H.L. Liu, J. H. Wu, J.H. Min, Tunable synthesis and multifunctionalities of Fe3O4-ZnO hybrid core-shell Nanocrystals, Mater. Res. Bull. 48 (2013) 551-558.

DOI: 10.1016/j.materresbull.2012.11.051

Google Scholar

[10] L. B. Scaffardi, N. Pellegri, Sizing gold nanoparticles by optical extinction spectroscopy, Nanotechnolol. 16 (2005) 158-163.

DOI: 10.1088/0957-4484/16/1/030

Google Scholar

[11] H.L. Liu, J.H. Wu, J.H. Min, Monosized core-shell Fe3O4(Fe)/Au muitifunctional nanocrystals, J. Nanosci. Nanotechnol. 9 (2009) 754-758.

Google Scholar