Interaction of V, Al, and N in Microalloyed Forging Steels after Hot Deformation

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A medium-carbon V-microalloyed steel (38MnSiVS5) with three different Al levels (0.006, 0.020, and 0.031 wt pct) was used to examine the interaction of V, Al, and N after hot deformation. A complete thermomechanical cycle was simulated in the laboratory using a Gleeble® 1500. Specimens were heated to a soaking temperature that varied from 1100 to 1250 °C for 5 or 45 min and control cooled to 1000 °C in 6 min, where they were compressed to 40 pct reduction at a strain rate of 1.0 s-1. After compression, the specimens were control cooled to 500 °C at 0.25 °C·s-1 and die quenched to room temperature. Additional specimens were processed without the compression step for comparison. The thermal and thermomechanically processed specimens were characterized by quantitative metallography and microhardness testing. The thermomechanically processed specimens with 0.006 wt pct Al maintained their hardness while reducing pearlite fraction by approximately 10 pct. The thermomechanical processed specimens with 0.020 and 0.031 wt pct Al showed a significant drop in microhardness and pearlite fractions, as compared to the thermal only processed specimens. The decrease in microhardness and pearlite fraction for the two higher-Al–containing alloys in both the thermal and thermomechanically processed specimens appears to follow the same linear trend, suggesting that AlN precipitation reduces the amount of N in solid solution, lowers the temperature at which V(C,N) precipitation occurs, and effectively reduces such strain-induced precipitation.

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604-609

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May 2014

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© 2014 Trans Tech Publications Ltd. All Rights Reserved

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[1] W. Morrison, "Overview of Microalloying in Steel," in The Use of Vanadium in Steel, Guilin, China, 2000, pp.25-35.

Google Scholar

[2] D. Naylor, "Microalloyed Forging Steels," Materials Science Forum, vol. 284-286, 1998, pp.83-94.

DOI: 10.4028/www.scientific.net/msf.284-286.83

Google Scholar

[3] M.D. Head, Ed., Bar Steels: Steel Products Manual, Warrendale, PA: Association for Iron and Steel Technology, 2010.

Google Scholar

[4] G. Krauss, Steels: Processing, Structure, and Performance, Materials Park, OH: ASM International, 2005.

Google Scholar

[5] T. Gladman, Grain Size Control, London, UK: Maney Publishing, 2004.

Google Scholar

[6] J. N. Cordea and R. E. Hook, "Recrystallization Behavior in Deformed Austenite of High Strength Low Alloy (HSLA) Steels," Metallurgical and Materials Transactions B, vol. 1, 1970, pp.111-118.

DOI: 10.1007/bf02819249

Google Scholar

[7] F. Wlison and T. Gladman, "Aluminum Nitride in Steel," International Materials Reviews, vol. 33, 1988, pp.221-286.

Google Scholar

[8] B. Mintz, "Influence of Nitrogen on Hot Ductility of Steels and Its Relationship to Problem of Transverse Cracking," Iron and Steelmaking, vol. 27, 2000, pp.343-347.

DOI: 10.1179/030192300677633

Google Scholar

[9] T. Gladman, The Physical Metallurgy of Microalloyed Steels. Institute of Materials, 1997.

Google Scholar

[10] T. N. Baker, "Processes, Microstructure and Properties of Vanadium Microalloyed Steels," Materials Science and Technology, vol. 25, 2009, pp.1083-1107.

DOI: 10.1179/174328409x453253

Google Scholar

[11] S. Zajac, "Precipitation of Microalloy Carbo-nitrides Prior, During, and After Austenite/Ferrite Transformation," Materials Science Forum, vol. 500-501, 2005, pp.75-86.

DOI: 10.4028/www.scientific.net/msf.500-501.75

Google Scholar

[12] S. Zajac, T. Siwecki, W.B. Hutchinson, and R. Lagneborg, "Strengthening Mechanisms in Vanadium Microalloyed Steels Intended for Long Products," ISIJ International, vol. 38, 1998, pp.1130-1139.

DOI: 10.2355/isijinternational.38.1130

Google Scholar

[13] X. Li, L. Zhao, X. Wang, and Y. Zhao, "Precipitation and Hetero-nucleation Effect of V(C,N) in V-microalloyed Steel," Journal of Wuhan University of Technology--Materials Science Edition, vol. 23, 2008, pp.844-849.

DOI: 10.1007/s11595-007-6844-x

Google Scholar

[14] S. Zajac, R. Lagneborg, and T. Siwecki, "The Role of Nitrogen in Microalloyed Steels," in Microalloying '95, Iron and Steel Society, 1995, pp.11-14.

Google Scholar

[15] L.M. Rothleutner, R. Cryderman, and C.J. Van Tyne, "Influence of Temperature and Holding Time on the Interaction of V, Al, and N in Microalloyed Forging Steels," Metallurgical and Materials Transactions A, accepted for publication pending minor revisions.

DOI: 10.1007/s11661-014-2375-1

Google Scholar

[16] B. Roebuck, J. D. Lord, M. Brooks, M. S. Loveday, C. M. Sellars, and R. W. Evans, "Measurement Good Practice Guide No. 3: Measuring Flow Stress in Hot Axisymmetric Compression Tests." National Physical Laboratory, 2002.

DOI: 10.1179/mht.2006.005

Google Scholar