Monomethyl β-Methylglutarate of New Synthetic Methods

Feng Wei He; Tong Liu; Ya Qin Zhang

doi:10.4028/www.scientific.net/AMR.960-961.134

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HomeAdvanced Materials ResearchAdvanced Materials Research Vols. 960-961Monomethyl β-Methylglutarate of New Synthetic...

Monomethyl β-Methylglutarate of New Synthetic Methods

Abstract:

Malonate ethyl ester of butene in the presence of sodium hydroxide was synthesized by addition reaction of 2-methyl propane-1,1,3 tricarboxylic acid ester, by hydrolysis decarboxylation heatingβ-methyl glutaric acid. First with excess of methanol into methyl metaplasiaβ-methyl dimethyl glutarate, and then itsβ-methyl glutaric acid methylation, get high yield of monomethyl β-methylglutarate.

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Periodical:

Advanced Materials Research (Volumes 960-961)

Pages:

134-137

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.960-961.134

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Online since:

June 2014

Authors:

Feng Wei He*, Tong Liu, Ya Qin Zhang

Keywords:

Butene Ethyl, Heteropoly Acid, Methyl Malonate, Monomethyl β-Methylglutarate, Musk Ketone

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