Low Temperature Oxidation Behaviors of CNTs/MoSi2 Composites

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Molybdenum disilicide (MoSi2) matrix composites with various contents of carbon nanotubes (CNTs) were fabricated by sintering in vacuum at 1550 °C for 1 h. The oxidation behaviors of CNTs/MoSi2 composites at 400 °C and 500 °C for 200 h in air were studied. Results showed that the weight loss of CNTs/MoSi2 composites increased with the increase of CNTs content. “Pest” phenomenon happened at 400 °C but not at 500 °C. Phase identification and microstructure of the samples were analyzed by X-ray diffraction (XRD) and scanning electron microscopy (SEM). It was found that many MoO3 whiskers and microcracks only occurred on the surface of CNTs/MoSi2 composites when oxidized at 400 °C in air, which leaded to the catastrophic disintegration of CNTs/MoSi2 composites.

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116-120

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June 2014

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© 2014 Trans Tech Publications Ltd. All Rights Reserved

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