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HomeJournal of Nano ResearchJournal of Nano Research Vol. 65Structure Evolution of La(OH)3 /Fe Composite...

Structure Evolution of La(OH)₃ /Fe Composite during Ball Milling

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Abstract:

Fe-10wt% La (OH)₃ composite powders have been fabricated by ball milling, under argon atmosphere for milling periods of 0, 5 and 10 h, respectively. Changes in structural, morphological, thermal and magnetic properties of the powders during mechanical alloying and during subsequent annealing have been examined by X-ray diffraction, scanning electron microscopy (SEM), differential scanning calorimetry (DSC) and vibrating sample magnetometer (VSM). XRD results: showed the formation of new phases (Fe and LaFeO3 perovskite) created through the ball milling. The results showed that the crystalline size of ball milled powders decreased with increasing the milling time. In fact, after 10 h of ball milling, La (OH)₃ changes from nanostructure in amorphous structure. The magnetic measurements display a distinct saturation magnetization and coercivity.

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Journal of Nano Research Vol. 65

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Periodical:

Journal of Nano Research (Volume 65)

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123-134

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https://doi.org/10.4028/www.scientific.net/JNanoR.65.123

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Online since:

December 2020

Authors:

Samira Lalaoua*, Bouguerra Bouzabata, Safia Alleg, Abedelmalik Djekoun, David Shmool

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Ball Milling, DRX, Lanthanum Oxide, ODS, SEM, VSM

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© 2020 Trans Tech Publications Ltd. All Rights Reserved

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