Investigation of Microstructure Evolution during AA6082 Chips Recycling through Friction Consolidation

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Abstract:

Recycling aluminum chips remains a major challenge in aluminum manufacturing because it is difficult to retain the original quality alloy properties while reducing the carbon footprint and ensuring a sustainable process. This work investigates the microstructural evolution and bonding quality of compacted AA6082 chips processed through friction extrusion/consolidation. The residual material left inside the extrusion container after processing at a high extrusion ratio was analyzed using SEM, EDS, and EBSD to understand bonding mechanisms and microstructure evolution in front of the die. The SEM results show that voids are still present between the chips in the initial compacted material which already shows bonding, while these voids are reducing towards the die interface, particularly related to the present severe plastic deformation. EDS analysis confirms the presence of Al (Fe,Mn)Si intermetallic particles, which break and disperse in the matrix because of shear deformation due to die rotation. EBSD analysis reveals that grains are coarser near the base material, and subdivisions of grains near the die interface are significant because of continuous dynamic recrystallization.

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[1] D. Raabe, D. Ponge, P.J. Uggowitzer, M. Roscher, M. Paolantonio, C. Liu, H. Antrekowitsch, E. Kozeschnik, D. Seidmann, B. Gault, F. De Geuser, A. Deschamps, C. Hutchinson, C. Liu, Z. Li, P. Prangnell, J. Robson, P. Shanthraj, S. Vakili, C. Sinclair, L. Bourgeois, and S. Pogatscher, Making sustainable aluminum by recycling scrap: The science of "dirty" alloys. Progress in Materials Science, 2022. 128: p.100947.

DOI: 10.1016/j.pmatsci.2022.100947

Google Scholar

[2] J. Gronostajski, J. Kaczmar, H. Marciniak, and A. Matuszak, Direct recycling of aluminium chips into extruded products. Journal of materials processing technology, 1997. 64(1-3): pp.149-156.

DOI: 10.1016/s0924-0136(96)02563-0

Google Scholar

[3] U.F. Suhuddin, L. Rath, R.M. Halak, and B. Klusemann, Microstructure evolution and texture development during production of homogeneous fine-grained aluminum wire by friction extrusion. Materials Characterization, 2023. 205: p.113252.

DOI: 10.1016/j.matchar.2023.113252

Google Scholar

[4] D. Baffari, A.P. Reynolds, A. Masnata, L. Fratini, and G. Ingarao, Friction stir extrusion to recycle aluminum alloys scraps: Energy efficiency characterization. Journal of Manufacturing Processes, 2019. 43: pp.63-69.

DOI: 10.1016/j.jmapro.2019.03.049

Google Scholar

[5] D. Baffari, G. Buffa, G. Ingarao, A. Masnata, and L. Fratini, Aluminium sheet metal scrap recycling through friction consolidation. Procedia Manufacturing, 2019. 29: pp.560-566.

DOI: 10.1016/j.promfg.2019.02.134

Google Scholar

[6] J. Lv, J. Yu, Z. Shi, W. Li, and J. Lin, Feasibility study of a novel multi-container extrusion method for manufacturing wide aluminium profiles with low force. Journal of Manufacturing Processes, 2023. 85: pp.584-593.

DOI: 10.1016/j.jmapro.2022.11.055

Google Scholar

[7] R.M. Halak, L. Rath, U.F. Suhuddin, J.F. dos Santos, and B. Klusemann, Changes in processing characteristics and microstructural evolution during friction extrusion of aluminum. International Journal of Material Forming, 2022. 15(3): p.24.

DOI: 10.1007/s12289-022-01670-y

Google Scholar

[8] W. Tang and A.P. Reynolds, Production of wire via friction extrusion of aluminum alloy machining chips. Journal of Materials Processing Technology, 2010. 210(15): pp.2231-2237.

DOI: 10.1016/j.jmatprotec.2010.08.010

Google Scholar

[9] P. Noga, A. Piotrowicz, T. Skrzekut, A. Zwoliński, and P. Strzępek, Effect of various forms of aluminum 6082 on the mechanical properties, microstructure and surface modification of the profile after extrusion process. Materials, 2021. 14(17): p.5066.

DOI: 10.3390/ma14175066

Google Scholar

[10] W. Tang and A.P. Reynolds, Friction consolidation of aluminum chips. Friction Stir Welding and Processing VI, 2011: pp.289-298.

DOI: 10.1002/9781118062302.ch34

Google Scholar

[11] G.Poy Ignacio, L. Rath, U.F. Suhuddin, and B. Klusemann, Friction extrusion from AlMgSi machining waste at high extrusion ratio. Materials Research Proceedings. 54.

DOI: 10.21741/9781644903599-79

Google Scholar

[12] M.K. Mejbel, S.K. Hussein, and I.T. Abdullah, Friction stir consolidation for recycling AA6061 chips with its metal flow investigation for billet production. Journal of Engineering Research, 2025. 13(2): pp.1170-1183.

DOI: 10.1016/j.jer.2024.04.010

Google Scholar

[13] R. Puleo, A. Latif, G. Ingarao, R. Di Lorenzo, and L. Fratini, Solid bonding criteria design for aluminum chips recycling through Friction Stir Consolidation. Journal of Materials Processing Technology, 2023. 319: p.118080.

DOI: 10.1016/j.jmatprotec.2023.118080

Google Scholar

[14] R. Puleo, A. Latif, G. Ingarao, and L. Fratini, A generalized parametric model for the bonding occurrence prediction in friction stir consolidation of aluminum alloys chips. Journal of Manufacturing Processes, 2024. 131: pp.604-618.

DOI: 10.1016/j.jmapro.2024.09.049

Google Scholar

[15] L. Rath, U.F. Suhuddin, and B. Klusemann, Comparison of friction extrusion processing from bulk and chips of aluminum-copper alloys. Key Engineering Materials, 2022. 926: pp.471-480.

DOI: 10.4028/p-vw04z5

Google Scholar

[16] C. Liu, Q. Du, N. Parson, and W.J. Poole, The interaction between Mn and Fe on the precipitation of Mn/Fe dispersoids in Al-Mg-Si-Mn-Fe alloys. Scripta Materialia, 2018. 152: pp.59-63.

DOI: 10.1016/j.scriptamat.2018.04.012

Google Scholar

[17] M.N. Rahaman, Ceramic processing and sintering. 2017: CRC press.

Google Scholar

[18] S. Gourdet and F. Montheillet, A model of continuous dynamic recrystallization. Acta Materialia, 2003. 51(9): pp.2685-2699.

DOI: 10.1016/s1359-6454(03)00078-8

Google Scholar

[19] H. McQueen, Development of dynamic recrystallization theory. Materials Science and Engineering: A, 2004. 387: pp.203-208.

Google Scholar