Hydrothermal Synthesis of Nano ZrO2 Powders

Cihangir Duran; Jia Yu; Kimiyasu Sato; Yuji Hotta; Koji Watari

doi:10.4028/www.scientific.net/KEM.317-318.195

Paper Titles

Influence of Nitride on Sinterability of the Composite of Lithium Aluminum Silicate and Silicon Carbide
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Hydrogen Reduction and Sintering Behavior of Al₂O₃/CuO Powder Mixtures Prepared from Different Raw Powders
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Low Cost Si₃N₄/SiC Nanocomposites, Processing, RT and HT Properties
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Fabrication of Si₃ N₄-TiN Nanocomposites via Various Routes
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Hydrothermal Synthesis of Nano ZrO₂ Powders
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Synthesis of Nanocrystalline α-Al₂O₃ Using a 2-Step Calcination Method
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Nano Magnetite Particles Prepared under the Combined Addition of Urea and Ammonia
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Synthesis of Nano-Scaled α-Al₂O₃ Particles by Combustion Spray Pyrolysis
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Synthesis of SiC Nano-Powders by Solid-Vapor Reaction
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HomeKey Engineering MaterialsKey Engineering Materials Vols. 317-318Hydrothermal Synthesis of Nano ZrO2 Powders

Hydrothermal Synthesis of Nano ZrO₂ Powders

Abstract:

Hydrothermal synthesis of nano ZrO2 powders were carried out at a temperature range of 100 to 200°C, using zirconium solution. Formation of ZrO2 formation was accelerated with temperature and precipitation of ZrO2 took place directly from the solution. XRD analysis revealed that monoclinic ZrO2 was formed at all conditions. Crystallite size was found to range from 2.6 to 4 nm. Mean particle size increased from 93 nm at 135°C to 125 nm at 200°C after reaction time of 2 h.

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Key Engineering Materials (Volumes 317-318)

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195-198

DOI:

https://doi.org/10.4028/www.scientific.net/KEM.317-318.195

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Online since:

August 2006

Authors:

Cihangir Duran, Jia Yu, Kimiyasu Sato, Yuji Hotta, Koji Watari

Keywords:

Hydrothermal Synthesis, Nanopowder, Zro₂

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References

[1] M. Yoshimura, S. Somiya: Materials Chemistry and Physics, 61 (1999) p.1.

Google Scholar

[2] W. Pyda, K. Haberko, and M. M. Bucko: Ceramics International, 18 (1992) p.321.

Google Scholar

[3] H-M. Cheng, L-J. Wu, J-M. Ma, Z-Y. Zhang and L-M. Qi: J. Euro. Cer. Soc. 19 (1999) p.1675.

Google Scholar

[4] T. Mitsuhashi, M. Ichihara and U. Tatsuke: J. Am. Ceram. Soc., 57 (1974) p.97.

Google Scholar

[5] J.H. Adair and R.P. Denkewicz: In Ceramic Transactions, Ceramic Power Science III, ed. G. L. Messing, American Ceramic Society, Westerville, OH, Vol. 12 (1990) p.25.

Google Scholar

[6] M.M.R. Boutz, R.J.M. Olde Scholtenhuis, A.J.A. Winnubst and A.J. Burggraaf: Mat. Res. Bull., Vol. 29 (1994), p.31.

DOI: 10.1016/0025-5408(94)90102-3

Google Scholar

[7] E. Tani, M. Yoshimura and S. Somiya: J. Am. Ceram. Soc., 66 (1983) pp.11-40 (111) - (111) (b) 4 6 15 0 20 40 60 80 100 0 0. 05 0. 1 0. 15 0. 2 0. 25 0. 3 Particle size, µm Cumulative Volume % (a) 4 6 15 2θ, Degrees.

Google Scholar