Some Problems on Evaluating Elastic Modulus of APSed Ceramic Top Coat for TBCs by Indentation Method


Article Preview

Elastic modulus of air plasma sprayed (APSed) YSZ (; ZrO2 stabilized by 8 wt. pct. Y2O3) top coat specimen, which is frequently used for thermal barrier coating (TBC) system for advanced gas turbines, was measured by employing the macro-, micro-, and nano-indentation methods. The elastic modulus was measured, following the Oliver-Pharr method. It was shown that the elastic modulus of the YSZ, as well as the microstructure, was significantly influenced by the spraying conditions employed. Especially the size of ceramic powders used was found to have the most pronounced effect. It was also shown that the elastic modulus revealed significant size effect: that is, there were significant differences in elastic modulus measured by the instruments on the macro-, micro-, and nano-levels. This size effect was discussed, correlating with some relating phenomena: crackings, sink-in, pile-up and spalling; as well as with the characteristic microstructures of the sprayed top coat.



Key Engineering Materials (Volumes 353-358)

Edited by:

Yu Zhou, Shan-Tung Tu and Xishan Xie




M. Okazaki and T. Ozaki, "Some Problems on Evaluating Elastic Modulus of APSed Ceramic Top Coat for TBCs by Indentation Method", Key Engineering Materials, Vols. 353-358, pp. 1802-1805, 2007

Online since:

September 2007




[1] R.A. Miller: J. Ame. Cer. Soc. Vol. 67 (1984), p.517.

[2] P.E. Hodge: J. Materials for Energy system Vol. 1 (1980), p.47.

[3] V.K. Tolpygo and K.S. Murphy: Metall. & Mater. Trans. Vol. 32A (2001), p.1467.

[4] M.Y. He, J.W. Hutchinson: Int. J. Solid Struc. Vol. 25 (1989), p.1053.

[5] A. Rabiei, A.G. Evans: Acta Mater. Vol. 48 (2000), p.3936.

[6] D.D. Hass, P.A. Parrish, H.N.G. Wadley: J. Vac. Sci. Tech. Vol. A16 (1998), p.3396.

[7] M. Gelll: Surface and Coating Tech. Vol. 177-178 (2004), p.97.

[8] M. Okazaki, T. Yoshida and A. Matsubara: J. Japan Inst. Metals Vol. 69 (2005), p.48.

[9] U. Schulz and W. Bunk, Z. Metallkd: Vol. 87 (1996), p.6.

[10] K. Wada, N. Yamaguchi and H. Matsubara: J. Cer. Soc. Japan Vol. 111 (2003), p.883 Penetration depth (μ m) 0 50 100 150 200 250 0 0. 5 1 1. 5 2 2. 5 3 3. 5 Elastic modulus ( GPa) Tensile test Cracking No cracking.

Fetching data from Crossref.
This may take some time to load.