Synthesis and Characterization the Intercalation Compound of SnS2-Ethylenediamine by Hydrothermal Reaction

Qing Lv; Cai Xia Li; Dan Yu Jiang; Qiang Li

doi:10.4028/www.scientific.net/KEM.512-515.215

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HomeKey Engineering MaterialsKey Engineering Materials Vols. 512-515Synthesis and Characterization the Intercalation...

Synthesis and Characterization the Intercalation Compound of SnS₂-Ethylenediamine by Hydrothermal Reaction

Abstract:

The intercalation of ethylenediamine (en) into SnS₂ was synthesised by hydrothermal reaction at the temperature of 180 °C.And then dispersed the intercalation compounds in N, N-dimethylformamide (DMF) by stirring 48h,getting a light yellow sol ,with the nature of uniform ,transparent and stable.Analysised the structural of the product by means of X-ray powder diffraction (XRD) .The morphology of sol was characterized by using of transmission electron microscopy (TEM).The UV-Vis spectrophotometer was utilized for the absorbance of the colloidal.The results show that en has been successfully inserted into the layer of tin disulphide,and the target products is of high purity and good crystal.The sol is of high stability and homogeneity, and have the strongest absorption at the Wavelength of 270nm.

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Periodical:

Key Engineering Materials (Volumes 512-515)

Pages:

215-218

DOI:

https://doi.org/10.4028/www.scientific.net/KEM.512-515.215

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Online since:

June 2012

Authors:

Qing Lv, Cai Xia Li, Dan Yu Jiang, Qiang Li

Keywords:

Ethylenediamine, Hydrothermal, Intercalation Compound, Tin Disulfide

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References

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