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HomeKey Engineering MaterialsKey Engineering Materials Vols. 602-603Synthesis and Analysis of Carbide-Derived Carbon...

Synthesis and Analysis of Carbide-Derived Carbon from TiC by Chlorination

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Abstract:

Carbide-derived carbons (CDCs) are produced from carbides by removing non-carbon elements in the process of selective etching. In this paper, CDC was prepared from TiC by chlorination at the temperature range of 600~1100°C. In the chlorinating process, carbide-derived carbon with different microstructure was obtained by controlling the reaction temperature. The structures of CDC were revealed with X-ray diffraction and Raman spectroscopy. The morphologies of CDC were analyzed by scanning electron microscope. From X-ray diffraction analysis, the CDC obtained from TiC in this experiment mainly consisted of amorphous carbon. Basing on scanning electron microscopy, carbide-derived carbon from TiC maintained the shape and size of TiC particles. Keywords: Carbide-derived carbons; chlorination; TiC

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High-Performance Ceramics VIII

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Periodical:

Key Engineering Materials (Volumes 602-603)

Pages:

463-466

DOI:

https://doi.org/10.4028/www.scientific.net/KEM.602-603.463

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Online since:

March 2014

Authors:

Jin Jia, Yuan Yuan Zhu, Ya Fei Zhang, Ruo Yu Chen, Bao Lin Xing, Ai Guo Zhou*

Keywords:

Carbide-Derived Carbons, Chlorination, TiC

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© 2014 Trans Tech Publications Ltd. All Rights Reserved

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