Optimization of Holding Time on Microwave Irradiation of the Composite Iron-Chromium Reinforced with Alumina Particle

Article Preview

Abstract:

In this study, the effect of holding time on the microwave sintered 84Fe-11Cr-5Al2O3 metal matrix composite (MMC) was investigated. Sintering was carried out in a tubular microwave furnace HAMiLab-V3 under N2 atmosphere. The holding time was selected between 0 to 75 minutes with increment of 15 minutes respectively. A study of microstructure and physical properties was carried out on sintered samples. It was discovered that, when the samples sintered at 1400oC with 20oC/min heating rate, the hardness was significantly increased from 110Hv to 160 Hv for holding time ranging from 30 to 45oC/min. Further increment until 75 minutes of holding time, no significant changes were obtained and hardness values were at steady state. The enhancement of bulk density and reduction of porosity were observed commences at 30 minutes until 45 minutes holding time. However, the results showed that the optimum holding time was at 45 minutes where the micro hardness is at the highest point which is about 160Hv.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

107-115

Citation:

Online since:

January 2016

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2016 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

* - Corresponding Author

[1] Y.V. Bykov, K.I. Rybakov, V.E. Semenov, J. Phys. D: Appl. Phys. 34 (2001) 55–75.

Google Scholar

[2] K.I. Rybakov, V.E. Semenov, S.V. Egorov, A.G. Eremeev, I.V. Plotnikov, Y.V. Bykov,J. Appl. Phys. 99 (2006) 023506.

Google Scholar

[3] W.L.E. Wong, M. Gupta, Adv. Eng. Mater. 9 (2007) 902–909.

Google Scholar

[4] Patterson MCL, Apte PS, Kimber RM, Roy R. Batch process for microwavesintering of Si3N4. Mater Res Soc Symp Proc1992. p.291–300.

Google Scholar

[5] Groover MP. Fundamentals of Modern Manufacturing. 2nd ed. USA: John wiley and Sons Inc; (2004).

Google Scholar

[6] Rao KJ, Ramesh PD. Use of microwaves for the synthesis and processing of materials, Bulletin of Material Science 1995; 18: 447.

Google Scholar

[7] Sunil BR, Sivaprahasam D, Subasri R. Microwave sintering of nanocrystalline WC-12Co: Challenges and perspectives. International Journal of Refractory Metals and Hard Materials. 2010; 28: 180-6.

DOI: 10.1016/j.ijrmhm.2009.08.005

Google Scholar

[8] Sutton WH. Microwave processing of ceramics. Am Ceram Soc Bull. 1989; 68: 376.

Google Scholar

[9] Janney MA, Kimrey HD, Schmidt MA, Kiggans JO. Grain growth in microwave-annealed alumina. J Am Ceram Soc. 1991; 74: 1675–81.

DOI: 10.1111/j.1151-2916.1991.tb07159.x

Google Scholar

[10] Tiegs TN, Kiggans JO, Kimrey HD. Microwavesintering of silicon nitride. Ceram Eng Sci Proc. 1991; 12: 1981–92.

Google Scholar

[11] Plucknett KP, Wilkinson DS. Microstructural characterization of microwave sintered silicon nitride ceramics. Mater Res Symp Proc. 1993; 245: 289–94.

Google Scholar

[12] Tiegs TN, Kiggans JO, Kimrey HD. Microwave processing of silicon nitride. Mater Res Symp Proc. 1990; 189: 267–72.

DOI: 10.1557/proc-189-267

Google Scholar

[13] Jones MI, Valecillos MC, Hirao K, Yamauchi Y. Grain growth in microwave sintered Si3N4 ceramics sintered from different starting powders. J Eur Ceram Soc. 2002; 22: 2981-8.

DOI: 10.1016/s0955-2219(02)00054-7

Google Scholar

[14] Chung-Hung Tam, Shih-Chin Lee, Shih-Hsien Chang, Fong-Cheng Tai, Effects of HIP Treatment on the Microstructure and Properties of Cr35-Si65 Target. Materials Transactions, Vol. 50, No. 2 (2009) 395-400.

DOI: 10.2320/matertrans.mer2008259

Google Scholar

[15] D. Agrawal, Latest global developments in microwave materials processing, Materials Research Innovations, Vol. 14, No. 1 (2010) 3-8.

DOI: 10.1179/143307510x12599329342926

Google Scholar

[16] S. Ramesh, C.Y. Tan, S.B. Bhaduri, W.D. Teng, Rapid densification of nanocrystalline hydroxyapatite for biomedical applications. Ceramics International, Vol. 33. No. 7 (2007) 1363-1367.

DOI: 10.1016/j.ceramint.2006.05.009

Google Scholar

[17] A. Mondal, A. Upadhyaya,D. Agrawal, Effect of heating mode and sintering temperature on the consolidation of 90W–7Ni–3Fe alloys,, Journal of Alloys and Compounds 509 (2011) 301–310.

DOI: 10.1016/j.jallcom.2010.09.008

Google Scholar

[18] S. Shamsuddin, J. B Shamsul, Z. Hussain, Z. A. Ahmad. Compaction study of particulate Iron-chromium matrix composite reinforced with alumina. In Proceedings of National Metallurgical Conference 2007, UTM & IMM.

Google Scholar

[19] W. Rahman, J. B Shamsul, M.N. Mazlee. Characterization and Optimization of Compaction Pressure in the Alumina Reinforced Iron-Chromium Composite under Microwave Sintering Process. In Proceedings of The 8th Asian-Australasian Conference on Composite Materials 2012, Kuala Lumpur.

DOI: 10.4028/www.scientific.net/kem.673.107

Google Scholar

[20] Martin J. M. and Castro F. Liquid Phase Sintering of P/M Aluminum Alloys: Effect of Processing Conditions, J. Mater. Process. Technol., vol. 143-144, (2003) pp.814-821.

DOI: 10.1016/s0924-0136(03)00335-2

Google Scholar

[21] Dudas L. and Dean W. A. The production of Precision Aluminum P/M Parts", Int. J. Powder Metall., vol. 5, pp.113-124. German R. M. "Sintering Theory and Practice., John Wiley Sons, Inc., New York, NJ, USA, (1996) pp.1-312.

Google Scholar

[22] Schaffer G. B., Hall B. J., Bonner S. J., Huo S. H. and Sercombe T. B. The Effect of the Atmosphere and the Role of Pore Filling on the Sintering of Aluminum, Acta Mater., vol. 54, (2006) pp.131-138.

DOI: 10.1016/j.actamat.2005.08.032

Google Scholar

[23] Hampshire S, Jack KH. The kinetics of densification and phase transformation of nitrogen ceramics. Proc Brit Ceram Soc. 31(1981) 37–49.

Google Scholar