Preparation and Oxidation Properties of Carbon/Carbon Composites with the Antioxidant SiC/NiCS Coating

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In the paper, the SiC/NiCS coating on carbon/carbon composites was designed and prepared, and its oxidation properties was investigated. The SiC transition layer is prepared by embedding method while the NiCS coating by brushing slurry. Oxidation resistance of various coatings and the same coating sintered by different ways are analyzed through the isothermal oxidation experiment. The strength retention of the samples after oxidation is tested through the three-point bending experiment. The surface and cross section morphology of the coating before and after oxidation are observed by SEM, and crystalline phases of the coating are analyzed by XRD. According to the results, the coating have excellent short-time oxidation resistance, and the weightless rate with oxidation time presents linear increasing trend basically. With the increase of temperature, the weight-loss rate increases. The more serious oxidation is, the lower bending strength retention rate is. The integrity and density of the barrier layer and the across-running cracks of the silicon carbide transition layer are the main factors influencing the oxidation resistance of the sample.

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881-888

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January 2017

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© 2017 Trans Tech Publications Ltd. All Rights Reserved

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[1] LI Cui-yun, LI Fu-an. Research of carbon/carbon composites' application[J]. New Chemical Materials, 2006 (3): 18-20. (in Chinese).

Google Scholar

[2] JIN Pei-peng. Potential aircraft engine materials-carbon/carbon composites[J]. Journal of Qinghai University, 2004, 22 (3): 18-20. (in Chinese).

Google Scholar

[3] YANG Wen-dong. Preparation and mechanism research of SiC/C-AlPO4 coated carbon/carbon composites[D]. Shaanxi University of Science and Technology, 2010. (in Chinese).

Google Scholar

[4] LI Yun-xin. Carbon/carbon composites[J]. Journal of Materials Science and Engineering, 1996, 14 (2): 6-14. (in Chinese).

Google Scholar

[5] YANG Hai-feng. Research about oxidation resistance of C/C composites in the high temperature[J]. Carbon Techniques, 2000, 111(6): 22-28. (in Chinese).

Google Scholar

[6] GUO Hai-ming. Preparation and performance of C/C composites with the anti-oxidation composite coating[J]. Aerospace Material Ttechnology, 1998(5): 37-40. (in Chinese).

Google Scholar

[7] S.J. Wu, L.F. Cheng, L.T. Zhang, et al. Oxidation behavior of 2D C/SiC with a multi-layer CVD SiC coating[J]. Surf. Coat. Technol., 2006, 200(14-15): 4489-4492.

DOI: 10.1016/j.surfcoat.2005.03.009

Google Scholar

[8] L.F. Cheng, Y.D. Xu, L.T. Zhang, et al. Thermal expansion and oxidation of 3D C/SiC composites with different coatings from room temperature to 1400℃[J]. Sci. Eng. Compos. Mater, 2002, 10(5): 377-382.

DOI: 10.1515/secm.2002.10.5.377

Google Scholar

[9] S.J. Wu, L.F. Cheng, L.T. Zhang, et al. Effect of CVD SiC coatings on oxidation behaviors of three dimensional C/SiC composites[J]. J. Inorg. Mater, 2005, 20(1): 251-256.

Google Scholar