DEM and Microstructure Analysis of Pure Molybdenum Powder Material during Equal Channel Angular Pressing

Article Preview

Abstract:

Pure molybdenum powder material was processed by equal channel angular pressing (ECAP) with different numbers of passes at the temperature of 400 °C and then Vickers microhardness measurements and scanning electron microscopy (SEM) analysis were conducted. The samples were further characterized with electron back scatter diffraction (EBSD) to examine the grain size. These experimental results exhibit that the powder material is well consolidated and the grains are refined by 2 passes of ECAP processing. In addition, discrete element method (DEM) was used to investigate the deformation behaviour of particles as well as the pores between the particles. The deformation of particles, the distribution of residual porosity and the variation of coordination number in pure molybdenum powder material sample during ECAP were obtained in microscopic scale and all the simulation results are well in line with the microstructure evolution.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

11-15

Citation:

Online since:

March 2017

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2017 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

[1] Luo Z.H. (2003) Application and development of molybdenum, China molybenum industry, 27(3), 17-20.

Google Scholar

[2] Wang D., Yuan X. and Li Z. (2006) Progress of research and applications for Mo metal and its alloys, Rare Metals Letters, 25(12): 1-7.

Google Scholar

[3] Valiev R.Z. and Langdon T.G. (2006) Principles of equal-channel angular pressing as a processing tool for grain refinement, Progress in Materials Science, 51(7): 881-981.

DOI: 10.1016/j.pmatsci.2006.02.003

Google Scholar

[4] Karaman I., Haouaoui M. and Maier H.J. (2007) Nanoparticle consolidation using euqal channel angular extrusion at room temperature, Jouranl of Materials Science, 42(5), 1561-1576.

DOI: 10.1007/s10853-006-0987-6

Google Scholar

[5] Wang X.X., Xue K.M. and Li P. (2010) Equal channel angular pressing and Torsion of pure aliminium powder in tubes, Advanced Materials Research, 97-101, 1109-1115.

DOI: 10.4028/www.scientific.net/amr.97-101.1109

Google Scholar

[6] Xue K.M., Wang X.X. and Li P. (2011) Numerical simulation and experiment of pure molybdenum powder sintered material with porosities during ECAP, The Chinese Journal of Nonferrous Metals, 21(1): 198-204.

Google Scholar

[7] Wang J., Li C.X. and Ruan X.Y. (2000) Mathematical model of powder metal compacting procrss based on modified ecperimental parameters, Journal of Shanghai Jiaotong University, 34(3), 322-325.

Google Scholar

[8] Wang Q. and Lu X.L. (2006) Numerical algorithm of discrite element method, Journal of Tong Ji University (natural science), 34(12): 1573-1577.

Google Scholar

[9] Li P., Wang X. and Xue K.M. (2013) Multi-scale study of pure molybdenum powder material in tubes during equal channel angular pressing, Materials Science and Engineering of Powder Metallurgy, 18(3), 452-458.

DOI: 10.4028/www.scientific.net/kem.732.11

Google Scholar

[10] Ruan J.M. and Huang P.Y. (2012) Principle of the powder metallurgy, China Machine Press.

Google Scholar