Briquetting Pressure Roles in Selective Reduction Process of Limonitic Nickel Laterite

Article Preview

Abstract:

Direct reduction is one of the methods used in nickel extraction from limonitic nickel laterite. Briquettes become an essential part of the direct reduction. This research examines the appropriate com-paction pressure of briquettes to achieve the optimum concentration, recovery of Ni and Fe, and selectivity factors also analyze the com-pounds formed. The briquettes were made at a pressure of 20 Kgf/cm2, 30 Kgf/cm2, 40 Kgf/cm2, and 50 Kgf/cm2. This study was performed out by mixing the prepared materials and then compact-ing them to form briquettes. Then, it was put into a crucible, and the coal-limestone bed mixture is added and put into the muffle fur-nace. Then, the direct reduction was started by heating at 700°C for 2 hours and continued at 1400°C for 6 hours. Next, it was continued with magnetic separation and weighing of the reduction products. The products were tested with SEM-EDX to determine the content. The products were tested with XRD to determine the compounds formed. The optimal results were obtained at variations of 30 Kgf/cm2 with a Ni content of 5.00% and Recovery of 86.76%.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

3-9

Citation:

Online since:

January 2023

Export:

Price:

Permissions CCC:

Permissions PLS:

Сopyright:

© 2023 Trans Tech Publications Ltd. All Rights Reserved

Share:

Citation:

* - Corresponding Author

[1] Abdul, F., Pintowantoro, S., Kawigraha, A., Nursidiq, A., Effects of reduction temperature to Ni and Fe content and the morphology of agglomerate of reduced laterite limonitic nickel ore by coal-bed method, AIP Conference Proceedings. 1945, 020034 (2018). https://doi.org/10.1063/1.5030256.

DOI: 10.1063/1.5030256

Google Scholar

[2] Pintowantoro, S., Widyartha, A.B., Setiyorini, Y., Abdul, F., Sodium Thiosulfate and Natural Sulfur: Novel Potential Additives for Selective Reduction of Limonitic Laterite Ore, Journal of Sustainable Metallurgy. 7 (2021) 481–494. https://doi.org/10.1007/s40831-021-00352-4.

DOI: 10.1007/s40831-021-00352-4

Google Scholar

[3] Šperl, J., Trčková, J., Permeability and porosity of rocks and their relationship based on laboratory testing, Acta Geodynamica et Geomaterialia. 5 (2008) 41–47.

Google Scholar

[4] Rabier, F., Temmerman, M., Böhm, T., Hartmann, H., Daugbjerg Jensen, P., Rathbauer, J., Carrasco, J., Fernández, M., Particle density determination of pellets and briquettes, Biomass and Bioenergy. 30 (2006) 954–963.

DOI: 10.1016/j.biombioe.2006.06.006

Google Scholar

[5] F. Abdul, S. Pintowantoro, Analysis of holding time variations to Ni and Fe content and morphology in nickel laterite limonitic reduction process by using coal-dolomite bed, AIP Conference Proceedings 1945, 020033 (2018), https://doi.org/10.1063/1.5030255.

DOI: 10.1063/1.5030255

Google Scholar

[6] Lemos, L.R., da Rocha, S.H.F.S., de Castro, L.F.A., Assunção, G.B.M., da Silva, G.L.R., Mechanical strength of briquettes for use in blast furnaces, Revista Escola de Minas. 72 (2019) 63–69. https://doi.org/10.1590/0370-44672017720156.

DOI: 10.1590/0370-44672017720156

Google Scholar

[7] Beheshti, R., Moosberg-Bustnes, J., Aune, R.E., Modeling and Simulation of Isothermal Reduction of a Single Hematite Pellet in Gas Mixtures of H2 and CO, TMS 2014: 143rd Annual Meeting & Exhibition. (2014) 495–502. https://doi.org/10.1007/978-3-319-48237-8_60.

DOI: 10.1007/978-3-319-48237-8_60

Google Scholar

[8] Elliott, R., Pickles, C.A., Forster, J., Thermodynamics of the Reduction Roasting of Nickeliferous Laterite Ores, Journal of Minerals and Materials Characterization and Engineering. 04 (2016) 320–346. https://doi.org/10.4236/jmmce.2016.46028.

DOI: 10.4236/jmmce.2016.46028

Google Scholar

[9] Jiang, M., Sun, T., Liu, Z., Kou, J., Liu, N., Zhang, S., Mechanism of sodium sulfate in promoting selective reduction of nickel laterite ore during reduction roasting process, International Journal of Mineral Processing. 123 (2013) 32–38.

DOI: 10.1016/j.minpro.2013.04.005

Google Scholar

[10] Morsi, I.M., El Barawy, K.A., Morsi, M.B., Abdel-Gawad, S.R., Silicothermic reduction of dolomite ore under inert atmosphere, Canadian Metallurgical Quarterly. 41 (2002) 15–28. https://doi.org/10.1179/cmq.2002.41.1.15.

DOI: 10.1179/cmq.2002.41.1.15

Google Scholar

[11] Chen, G.J., Shiau, J.S., Liu, S.H., Hwang, W.S., Optimal combination of calcination and reduction conditions as well as Na2SO4 additive for carbothermic reduction of limonite ore, Materials Transactions, 57 (2016) 1560–1566.

DOI: 10.2320/matertrans.m2016072

Google Scholar

[12] Li, G., Shi, T., Rao, M., Jiang, T., Zhang, Y., Beneficiation of nickeliferous laterite by reduction roasting in the presence of sodium sulfate, Minerals Engineering. 32 (2012) 19–26. https://doi.org/10.1016/j.mineng.2012.03.012.

DOI: 10.1016/j.mineng.2012.03.012

Google Scholar

[13] Setiawan, I., Febrina, E., Subagja, R., Harjanto, S., Firdiyono, F., Investigations on mineralogical characteristics of Indonesian nickel laterite ores during the roasting process, IOP Conference Series: Materials Science and Engineering. 541 (2019).

DOI: 10.1088/1757-899x/541/1/012038

Google Scholar

[14] Li, Q., Wei, Y., Li, B., Zhou, S., Wang, H., Ma, B., Wang, C., Phase transformation in magnesium-rich nickel oxide ore after reduction roasting process, TMS Annual Meeting. 2015-March, (2015) 297–304.

DOI: 10.1007/978-3-319-48217-0_38

Google Scholar

[15] Kambuna, B.N.H., Triana, T., Supriyatna, Y.I., Analysis of metal phase transformation and particle growth of the reduction ferronickel plant dust pellet in variations temperature. PROCEEDINGS OF THE 3RD INTERNATIONAL SEMINAR ON METALLURGY AND MATERIALS (ISMM2019): Exploring New Innovation in Metallurgy and Materials. 2232, 060005 (2020).

DOI: 10.1063/5.0001935

Google Scholar

[16] F. Abdul, S. Pintowantoro, A.B. Hidayatullah, Analysis of Cylindrical Briquette Dimension on Total Iron Content and the Degree of Metallization in Direct Reduction Process of Iron Ore and Iron Sand Mixture, Materials Science Forum. 964 (2019) 19–25. https://doi.org/10.4028/www.scientific.net/msf.964.19.

DOI: 10.4028/www.scientific.net/msf.964.19

Google Scholar